Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide

In the title compound, C(22)H(27)N(2)O(2), the piperidine ring adopts a half-chair conformation with the benzene rings inclined in a trans orientation with respect to the piperidine ring [dihedral angle between the benzene rings = 89.1 (1)°]. In the crystal, a three-centre asymmetric N—H⋯O/C—H⋯O hyd...

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Detalles Bibliográficos
Autores principales: Prathebha, K., Reuben Jonathan, D., Sathya, S., Vasanthi, R., Usha, G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257237/
https://www.ncbi.nlm.nih.gov/pubmed/25484801
http://dx.doi.org/10.1107/S1600536814021965
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author Prathebha, K.
Reuben Jonathan, D.
Sathya, S.
Vasanthi, R.
Usha, G.
author_facet Prathebha, K.
Reuben Jonathan, D.
Sathya, S.
Vasanthi, R.
Usha, G.
author_sort Prathebha, K.
collection PubMed
description In the title compound, C(22)H(27)N(2)O(2), the piperidine ring adopts a half-chair conformation with the benzene rings inclined in a trans orientation with respect to the piperidine ring [dihedral angle between the benzene rings = 89.1 (1)°]. In the crystal, a three-centre asymmetric N—H⋯O/C—H⋯O hydrogen-bonding inter­action leads to the formation of chains extending along the a-axis direction.
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spelling pubmed-42572372014-12-05 Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide Prathebha, K. Reuben Jonathan, D. Sathya, S. Vasanthi, R. Usha, G. Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(22)H(27)N(2)O(2), the piperidine ring adopts a half-chair conformation with the benzene rings inclined in a trans orientation with respect to the piperidine ring [dihedral angle between the benzene rings = 89.1 (1)°]. In the crystal, a three-centre asymmetric N—H⋯O/C—H⋯O hydrogen-bonding inter­action leads to the formation of chains extending along the a-axis direction. International Union of Crystallography 2014-10-15 /pmc/articles/PMC4257237/ /pubmed/25484801 http://dx.doi.org/10.1107/S1600536814021965 Text en © Prathebha et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Prathebha, K.
Reuben Jonathan, D.
Sathya, S.
Vasanthi, R.
Usha, G.
Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title_full Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title_fullStr Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title_full_unstemmed Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title_short Crystal structure of 4-methyl-N-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
title_sort crystal structure of 4-methyl-n-{[1-(4-methyl­benzo­yl)piperidin-4-yl]meth­yl}benzamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257237/
https://www.ncbi.nlm.nih.gov/pubmed/25484801
http://dx.doi.org/10.1107/S1600536814021965
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