Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide

In the title compound, C(12)H(11)N(3)O(2)S, the dihedral angle between the 4H-chromen-4-one ring system and the –CH=N—NH—CS—NH– unit is 6.22 (1)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(14) loops. The dimers are reinforced by a pair of C—H⋯O inter...

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Autores principales: Vimala, G., Govindaraj, J., Haribabu, J., Karvembu, R., SubbiahPandi, A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257262/
https://www.ncbi.nlm.nih.gov/pubmed/25484795
http://dx.doi.org/10.1107/S1600536814021667
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author Vimala, G.
Govindaraj, J.
Haribabu, J.
Karvembu, R.
SubbiahPandi, A.
author_facet Vimala, G.
Govindaraj, J.
Haribabu, J.
Karvembu, R.
SubbiahPandi, A.
author_sort Vimala, G.
collection PubMed
description In the title compound, C(12)H(11)N(3)O(2)S, the dihedral angle between the 4H-chromen-4-one ring system and the –CH=N—NH—CS—NH– unit is 6.22 (1)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(14) loops. The dimers are reinforced by a pair of C—H⋯O inter­actions, which generate R (2) (2)(10) loops.
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spelling pubmed-42572622014-12-05 Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide Vimala, G. Govindaraj, J. Haribabu, J. Karvembu, R. SubbiahPandi, A. Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(12)H(11)N(3)O(2)S, the dihedral angle between the 4H-chromen-4-one ring system and the –CH=N—NH—CS—NH– unit is 6.22 (1)°. In the crystal, inversion dimers linked by pairs of N—H⋯O hydrogen bonds generate R (2) (2)(14) loops. The dimers are reinforced by a pair of C—H⋯O inter­actions, which generate R (2) (2)(10) loops. International Union of Crystallography 2014-10-08 /pmc/articles/PMC4257262/ /pubmed/25484795 http://dx.doi.org/10.1107/S1600536814021667 Text en © Vimala et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Vimala, G.
Govindaraj, J.
Haribabu, J.
Karvembu, R.
SubbiahPandi, A.
Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title_full Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title_fullStr Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title_full_unstemmed Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title_short Crystal structure of (2E)-N-methyl-2-[(4-oxo-4H-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
title_sort crystal structure of (2e)-n-methyl-2-[(4-oxo-4h-chromen-3-yl)methyl­idene]hydrazine­carbo­thio­amide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257262/
https://www.ncbi.nlm.nih.gov/pubmed/25484795
http://dx.doi.org/10.1107/S1600536814021667
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