Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione

The title compound, C(26)H(20)O(5), crystallizes with two independent molecules (A and B) in the asymmetric unit, which differ primarily in the location of the –OCH(3) groups. In the crystal, the mol­ecules form a layered structure parallel to (10-1) by C—H⋯O hydrogen-bonded networks. Adjacent layer...

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Detalles Bibliográficos
Autores principales: Sooksimuang, Thanasat, Kamtonwong, Siriporn, Parnchan, Waraporn, Kangkaew, Laongdao, Sahasithiwat, Somboon
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257283/
https://www.ncbi.nlm.nih.gov/pubmed/25484762
http://dx.doi.org/10.1107/S1600536814023137
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author Sooksimuang, Thanasat
Kamtonwong, Siriporn
Parnchan, Waraporn
Kangkaew, Laongdao
Sahasithiwat, Somboon
author_facet Sooksimuang, Thanasat
Kamtonwong, Siriporn
Parnchan, Waraporn
Kangkaew, Laongdao
Sahasithiwat, Somboon
author_sort Sooksimuang, Thanasat
collection PubMed
description The title compound, C(26)H(20)O(5), crystallizes with two independent molecules (A and B) in the asymmetric unit, which differ primarily in the location of the –OCH(3) groups. In the crystal, the mol­ecules form a layered structure parallel to (10-1) by C—H⋯O hydrogen-bonded networks. Adjacent layers are also linked by further C—H⋯O hydrogen bonds, forming a three-dimensional structure.
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spelling pubmed-42572832014-12-05 Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione Sooksimuang, Thanasat Kamtonwong, Siriporn Parnchan, Waraporn Kangkaew, Laongdao Sahasithiwat, Somboon Acta Crystallogr Sect E Struct Rep Online Research Communications The title compound, C(26)H(20)O(5), crystallizes with two independent molecules (A and B) in the asymmetric unit, which differ primarily in the location of the –OCH(3) groups. In the crystal, the mol­ecules form a layered structure parallel to (10-1) by C—H⋯O hydrogen-bonded networks. Adjacent layers are also linked by further C—H⋯O hydrogen bonds, forming a three-dimensional structure. International Union of Crystallography 2014-10-29 /pmc/articles/PMC4257283/ /pubmed/25484762 http://dx.doi.org/10.1107/S1600536814023137 Text en © Sooksimuang et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Sooksimuang, Thanasat
Kamtonwong, Siriporn
Parnchan, Waraporn
Kangkaew, Laongdao
Sahasithiwat, Somboon
Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title_full Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title_fullStr Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title_full_unstemmed Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title_short Crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
title_sort crystal structure of 3,13-dimethoxy-5,6,10,11-tetrahydrofuro[3,4-i][5]helicene-7,9-dione
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257283/
https://www.ncbi.nlm.nih.gov/pubmed/25484762
http://dx.doi.org/10.1107/S1600536814023137
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