Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one

The asymmetric unit of the title compound, C(10)H(14)N(2)O(3), contains two independent mol­ecules with similar conformations. In the both mol­ecules, the cyclo­hexene rings adopt the same envelope conformation with the flap C atoms lying 0.658 (3) and 0.668 (3) Å from the mean planes formed by the...

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Autores principales: Vigante, Brigita, Stepanovs, Dmitrijs, Pelss, Andrejs, Mishnev, Anatoly
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257328/
https://www.ncbi.nlm.nih.gov/pubmed/25484751
http://dx.doi.org/10.1107/S1600536814023009
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author Vigante, Brigita
Stepanovs, Dmitrijs
Pelss, Andrejs
Mishnev, Anatoly
author_facet Vigante, Brigita
Stepanovs, Dmitrijs
Pelss, Andrejs
Mishnev, Anatoly
author_sort Vigante, Brigita
collection PubMed
description The asymmetric unit of the title compound, C(10)H(14)N(2)O(3), contains two independent mol­ecules with similar conformations. In the both mol­ecules, the cyclo­hexene rings adopt the same envelope conformation with the flap C atoms lying 0.658 (3) and 0.668 (3) Å from the mean planes formed by the remaining atoms. In the crystal, adjacent mol­ecules are connected via N—H⋯O hydrogen bonds and weak C—H⋯O inter­actions, forming supra­molecular layers parallel to (-101).
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spelling pubmed-42573282014-12-05 Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one Vigante, Brigita Stepanovs, Dmitrijs Pelss, Andrejs Mishnev, Anatoly Acta Crystallogr Sect E Struct Rep Online Research Communications The asymmetric unit of the title compound, C(10)H(14)N(2)O(3), contains two independent mol­ecules with similar conformations. In the both mol­ecules, the cyclo­hexene rings adopt the same envelope conformation with the flap C atoms lying 0.658 (3) and 0.668 (3) Å from the mean planes formed by the remaining atoms. In the crystal, adjacent mol­ecules are connected via N—H⋯O hydrogen bonds and weak C—H⋯O inter­actions, forming supra­molecular layers parallel to (-101). International Union of Crystallography 2014-10-24 /pmc/articles/PMC4257328/ /pubmed/25484751 http://dx.doi.org/10.1107/S1600536814023009 Text en © Vigante et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Vigante, Brigita
Stepanovs, Dmitrijs
Pelss, Andrejs
Mishnev, Anatoly
Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title_full Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title_fullStr Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title_full_unstemmed Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title_short Crystal structure of 3-amino-5,5-dimethyl-2-[(E)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
title_sort crystal structure of 3-amino-5,5-dimethyl-2-[(e)-2-nitro­ethen­yl]cyclo­hex-2-en-1-one
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257328/
https://www.ncbi.nlm.nih.gov/pubmed/25484751
http://dx.doi.org/10.1107/S1600536814023009
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