Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide

In the title compound, C(13)H(10)BrNO(2), the mean plane of the non-H atoms of the central amide C—N—C(=O)—C fragment (r.m.s. deviation = 0.004 Å) forms a dihedral angle of 73.97 (12)° with the hy­droxy-substituted benzene ring and 25.42 (19)° with the bromo-substituted benzene ring. The two aromati...

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Autores principales: Moreno-Fuquen, Rodolfo, Melo, Vanessa, Ellena, Javier
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257397/
https://www.ncbi.nlm.nih.gov/pubmed/25553033
http://dx.doi.org/10.1107/S1600536814024696
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author Moreno-Fuquen, Rodolfo
Melo, Vanessa
Ellena, Javier
author_facet Moreno-Fuquen, Rodolfo
Melo, Vanessa
Ellena, Javier
author_sort Moreno-Fuquen, Rodolfo
collection PubMed
description In the title compound, C(13)H(10)BrNO(2), the mean plane of the non-H atoms of the central amide C—N—C(=O)—C fragment (r.m.s. deviation = 0.004 Å) forms a dihedral angle of 73.97 (12)° with the hy­droxy-substituted benzene ring and 25.42 (19)° with the bromo-substituted benzene ring. The two aromatic rings are inclined to one another by 80.7 (2)°. In the crystal, mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds, forming chains along [010]. The chains are linked by weak C—H⋯O hydrogen bonds, forming sheets parallel to (100), and enclosing R (3) (3)(17) and R (3) (2)(9) ring motifs.
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spelling pubmed-42573972014-12-31 Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide Moreno-Fuquen, Rodolfo Melo, Vanessa Ellena, Javier Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(13)H(10)BrNO(2), the mean plane of the non-H atoms of the central amide C—N—C(=O)—C fragment (r.m.s. deviation = 0.004 Å) forms a dihedral angle of 73.97 (12)° with the hy­droxy-substituted benzene ring and 25.42 (19)° with the bromo-substituted benzene ring. The two aromatic rings are inclined to one another by 80.7 (2)°. In the crystal, mol­ecules are linked by O—H⋯O and N—H⋯O hydrogen bonds, forming chains along [010]. The chains are linked by weak C—H⋯O hydrogen bonds, forming sheets parallel to (100), and enclosing R (3) (3)(17) and R (3) (2)(9) ring motifs. International Union of Crystallography 2014-11-15 /pmc/articles/PMC4257397/ /pubmed/25553033 http://dx.doi.org/10.1107/S1600536814024696 Text en © Moreno-Fuquen et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Moreno-Fuquen, Rodolfo
Melo, Vanessa
Ellena, Javier
Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title_full Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title_fullStr Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title_full_unstemmed Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title_short Crystal structure of 4-bromo-N-(2-hydroxy­phen­yl)benzamide
title_sort crystal structure of 4-bromo-n-(2-hydroxy­phen­yl)benzamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257397/
https://www.ncbi.nlm.nih.gov/pubmed/25553033
http://dx.doi.org/10.1107/S1600536814024696
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