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Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione
In the title compound, C(18)H(17)N(3)O(3), the dihedral angle between the planes of the indazole ring system [maximum deviation = 0.012 (1) Å] and the pyran-2,4-dione ring is 54.03 (6)°. An intramolecular N—H⋯O hydrogen bond closes an S(6) ring. The same H atom also participates in an intermolecul...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2014
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257434/ https://www.ncbi.nlm.nih.gov/pubmed/25553030 http://dx.doi.org/10.1107/S1600536814024520 |
| _version_ | 1782347750818447360 |
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| author | El Ghozlani, Mohamed Rakib, El Mostapha Gamouh, Ahmed Saadi, Mohamed El Ammari, Lahcen |
| author_facet | El Ghozlani, Mohamed Rakib, El Mostapha Gamouh, Ahmed Saadi, Mohamed El Ammari, Lahcen |
| author_sort | El Ghozlani, Mohamed |
| collection | PubMed |
| description | In the title compound, C(18)H(17)N(3)O(3), the dihedral angle between the planes of the indazole ring system [maximum deviation = 0.012 (1) Å] and the pyran-2,4-dione ring is 54.03 (6)°. An intramolecular N—H⋯O hydrogen bond closes an S(6) ring. The same H atom also participates in an intermolecular N—H⋯O hydrogen bond, which generates an inversion dimer. The dimers are linked by weak C—H⋯O contacts, thereby forming a three-dimensional network. |
| format | Online Article Text |
| id | pubmed-4257434 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2014 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-42574342014-12-31 Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione El Ghozlani, Mohamed Rakib, El Mostapha Gamouh, Ahmed Saadi, Mohamed El Ammari, Lahcen Acta Crystallogr Sect E Struct Rep Online Data Reports In the title compound, C(18)H(17)N(3)O(3), the dihedral angle between the planes of the indazole ring system [maximum deviation = 0.012 (1) Å] and the pyran-2,4-dione ring is 54.03 (6)°. An intramolecular N—H⋯O hydrogen bond closes an S(6) ring. The same H atom also participates in an intermolecular N—H⋯O hydrogen bond, which generates an inversion dimer. The dimers are linked by weak C—H⋯O contacts, thereby forming a three-dimensional network. International Union of Crystallography 2014-11-15 /pmc/articles/PMC4257434/ /pubmed/25553030 http://dx.doi.org/10.1107/S1600536814024520 Text en © El Ghozlani et al. 2014 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Data Reports El Ghozlani, Mohamed Rakib, El Mostapha Gamouh, Ahmed Saadi, Mohamed El Ammari, Lahcen Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title | Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title_full | Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title_fullStr | Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title_full_unstemmed | Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title_short | Crystal structure of 3-{1-[(1-allyl-1H-indazol-6-yl)amino]ethylidene}-6-methyl-2H-pyran-2,4(3H)-dione |
| title_sort | crystal structure of 3-{1-[(1-allyl-1h-indazol-6-yl)amino]ethylidene}-6-methyl-2h-pyran-2,4(3h)-dione |
| topic | Data Reports |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257434/ https://www.ncbi.nlm.nih.gov/pubmed/25553030 http://dx.doi.org/10.1107/S1600536814024520 |
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