The optimization of essential oils supercritical CO(2) extraction from Lavandula hybrida through static-dynamic steps procedure and semi-continuous technique using response surface method

AIM: The aim of this study was to examine and evaluate crucial variables in essential oils extraction process from Lavandula hybrida through static-dynamic and semi-continuous techniques using response surface method. MATERIALS AND METHODS: Essential oil components were extracted from Lavandula hybrida (Lavandin) flowers using supercritical carbon dioxide via static-dynamic steps (SDS) procedure, and semi-continuous (SC) technique. RESULTS: Using response surface method the optimum extraction yield (4.768%) was obtained via SDS at 108.7 bar, 48.5°C, 120 min (static: 8×15), 24 min (dynamic: 8×3 min) in contrast to the 4.620% extraction yield for the SC at 111.6 bar, 49.2°C, 14 min (static), 121.1 min (dynamic). CONCLUSION: The results indicated that a substantial reduction (81.56%) solvent usage (kg CO(2)/g oil) is observed in the SDS method versus the conventional SC method.