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GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
OBJECTIVE: This study evaluated the glass transition temperature (T(g)) and degree of conversion (DC) of a light-cured (Fill Magic) versus a chemically cured (Concise) orthodontic composite. MATERIAL AND METHODS: Anelastic relaxation spectroscopy was used for the first time to determine the T(g) of...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Faculdade de Odontologia de Bauru da Universidade de São Paulo
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4327515/ https://www.ncbi.nlm.nih.gov/pubmed/20027428 http://dx.doi.org/10.1590/S1678-77572009000600006 |
Sumario: | OBJECTIVE: This study evaluated the glass transition temperature (T(g)) and degree of conversion (DC) of a light-cured (Fill Magic) versus a chemically cured (Concise) orthodontic composite. MATERIAL AND METHODS: Anelastic relaxation spectroscopy was used for the first time to determine the T(g) of a dental composite, while the DC was evaluated by infrared spectroscopy. The light-cured composite specimens were irradiated with a commercial LED light-curing unit using different exposure times (40, 90 and 120 s). RESULTS: Fill Magic presented lower T(g) than Concise (35-84°C versus 135°C), but reached a higher DC. CONCLUSIONS: The results of this study suggest that Fill Magic has lower T(g) than Concise due to its higher organic phase content, and that when this light-cured composite is used to bond orthodontic brackets, a minimum energy density of 7.8 J/cm(2) is necessary to reach adequate conversion level and obtain satisfactory adhesion. |
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