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GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE

OBJECTIVE: This study evaluated the glass transition temperature (T(g)) and degree of conversion (DC) of a light-cured (Fill Magic) versus a chemically cured (Concise) orthodontic composite. MATERIAL AND METHODS: Anelastic relaxation spectroscopy was used for the first time to determine the T(g) of...

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Autores principales: Sostena, Michela M. D. S., Nogueira, Renata A., Grandini, Carlos R., Moraes, João Carlos Silos
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Faculdade de Odontologia de Bauru da Universidade de São Paulo 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4327515/
https://www.ncbi.nlm.nih.gov/pubmed/20027428
http://dx.doi.org/10.1590/S1678-77572009000600006
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author Sostena, Michela M. D. S.
Nogueira, Renata A.
Grandini, Carlos R.
Moraes, João Carlos Silos
author_facet Sostena, Michela M. D. S.
Nogueira, Renata A.
Grandini, Carlos R.
Moraes, João Carlos Silos
author_sort Sostena, Michela M. D. S.
collection PubMed
description OBJECTIVE: This study evaluated the glass transition temperature (T(g)) and degree of conversion (DC) of a light-cured (Fill Magic) versus a chemically cured (Concise) orthodontic composite. MATERIAL AND METHODS: Anelastic relaxation spectroscopy was used for the first time to determine the T(g) of a dental composite, while the DC was evaluated by infrared spectroscopy. The light-cured composite specimens were irradiated with a commercial LED light-curing unit using different exposure times (40, 90 and 120 s). RESULTS: Fill Magic presented lower T(g) than Concise (35-84°C versus 135°C), but reached a higher DC. CONCLUSIONS: The results of this study suggest that Fill Magic has lower T(g) than Concise due to its higher organic phase content, and that when this light-cured composite is used to bond orthodontic brackets, a minimum energy density of 7.8 J/cm(2) is necessary to reach adequate conversion level and obtain satisfactory adhesion.
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spelling pubmed-43275152015-04-17 GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE Sostena, Michela M. D. S. Nogueira, Renata A. Grandini, Carlos R. Moraes, João Carlos Silos J Appl Oral Sci Original Article OBJECTIVE: This study evaluated the glass transition temperature (T(g)) and degree of conversion (DC) of a light-cured (Fill Magic) versus a chemically cured (Concise) orthodontic composite. MATERIAL AND METHODS: Anelastic relaxation spectroscopy was used for the first time to determine the T(g) of a dental composite, while the DC was evaluated by infrared spectroscopy. The light-cured composite specimens were irradiated with a commercial LED light-curing unit using different exposure times (40, 90 and 120 s). RESULTS: Fill Magic presented lower T(g) than Concise (35-84°C versus 135°C), but reached a higher DC. CONCLUSIONS: The results of this study suggest that Fill Magic has lower T(g) than Concise due to its higher organic phase content, and that when this light-cured composite is used to bond orthodontic brackets, a minimum energy density of 7.8 J/cm(2) is necessary to reach adequate conversion level and obtain satisfactory adhesion. Faculdade de Odontologia de Bauru da Universidade de São Paulo 2009-12 /pmc/articles/PMC4327515/ /pubmed/20027428 http://dx.doi.org/10.1590/S1678-77572009000600006 Text en http://creativecommons.org/licenses/by-nc/3.0/ This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Original Article
Sostena, Michela M. D. S.
Nogueira, Renata A.
Grandini, Carlos R.
Moraes, João Carlos Silos
GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title_full GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title_fullStr GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title_full_unstemmed GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title_short GLASS TRANSITION AND DEGREE OF CONVERSION OF A LIGHT-CURED ORTHODONTIC COMPOSITE
title_sort glass transition and degree of conversion of a light-cured orthodontic composite
topic Original Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4327515/
https://www.ncbi.nlm.nih.gov/pubmed/20027428
http://dx.doi.org/10.1590/S1678-77572009000600006
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