Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide

In the crystal structure of the title compound, C(11)H(14)N(2)OS, the six atoms of the central C(2)N(2)OS residue are coplanar (r.m.s. deviation = 0.002 Å), which facilitates the formation of an intra­molecular N—H⋯O hydrogen bond, which closes an S(6) loop. The terminal phenyl ring is inclined with...

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Autores principales: Jasinski, Jerry P., Akkurt, Mehmet, Mohamed, Shaaban K., Gad, Mohamed A., Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4331893/
https://www.ncbi.nlm.nih.gov/pubmed/25705507
http://dx.doi.org/10.1107/S2056989014027133
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author Jasinski, Jerry P.
Akkurt, Mehmet
Mohamed, Shaaban K.
Gad, Mohamed A.
Albayati, Mustafa R.
author_facet Jasinski, Jerry P.
Akkurt, Mehmet
Mohamed, Shaaban K.
Gad, Mohamed A.
Albayati, Mustafa R.
author_sort Jasinski, Jerry P.
collection PubMed
description In the crystal structure of the title compound, C(11)H(14)N(2)OS, the six atoms of the central C(2)N(2)OS residue are coplanar (r.m.s. deviation = 0.002 Å), which facilitates the formation of an intra­molecular N—H⋯O hydrogen bond, which closes an S(6) loop. The terminal phenyl ring is inclined with respect to the central plane [dihedral angle = 42.10 (6)°]. The most prominent feature of the crystal packing is the formation of {⋯HNCS}(2) synthons resulting in centrosymmetric dimers.
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spelling pubmed-43318932015-02-20 Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide Jasinski, Jerry P. Akkurt, Mehmet Mohamed, Shaaban K. Gad, Mohamed A. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the crystal structure of the title compound, C(11)H(14)N(2)OS, the six atoms of the central C(2)N(2)OS residue are coplanar (r.m.s. deviation = 0.002 Å), which facilitates the formation of an intra­molecular N—H⋯O hydrogen bond, which closes an S(6) loop. The terminal phenyl ring is inclined with respect to the central plane [dihedral angle = 42.10 (6)°]. The most prominent feature of the crystal packing is the formation of {⋯HNCS}(2) synthons resulting in centrosymmetric dimers. International Union of Crystallography 2015-01-01 /pmc/articles/PMC4331893/ /pubmed/25705507 http://dx.doi.org/10.1107/S2056989014027133 Text en © Jasinski et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Jasinski, Jerry P.
Akkurt, Mehmet
Mohamed, Shaaban K.
Gad, Mohamed A.
Albayati, Mustafa R.
Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title_full Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title_fullStr Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title_full_unstemmed Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title_short Crystal structure of N-(propan-2-yl­carbamo­thio­yl)benzamide
title_sort crystal structure of n-(propan-2-yl­carbamo­thio­yl)benzamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4331893/
https://www.ncbi.nlm.nih.gov/pubmed/25705507
http://dx.doi.org/10.1107/S2056989014027133
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