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Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide
In the title compound, C(9)H(9)ClN(4)OS, the dihedral angle between the acetamide moiety and the pyridine ring is 4.83 (12)°. The O=C—C—Cl torsion angle is 46.4 (3)° and an intramolecular C—H⋯O interaction generates an S(6) ring. In the crystal, molecules are linked by N—H⋯O, N—H⋯N and C—H⋯N hydr...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2015
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4350726/ https://www.ncbi.nlm.nih.gov/pubmed/25844231 http://dx.doi.org/10.1107/S2056989015002431 |
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| author | Mohamed, Shaaban K. Knight, Kyle S. Akkurt, Mehmet Hussein, Bahgat R. M. Albayati, Mustafa R. |
| author_facet | Mohamed, Shaaban K. Knight, Kyle S. Akkurt, Mehmet Hussein, Bahgat R. M. Albayati, Mustafa R. |
| author_sort | Mohamed, Shaaban K. |
| collection | PubMed |
| description | In the title compound, C(9)H(9)ClN(4)OS, the dihedral angle between the acetamide moiety and the pyridine ring is 4.83 (12)°. The O=C—C—Cl torsion angle is 46.4 (3)° and an intramolecular C—H⋯O interaction generates an S(6) ring. In the crystal, molecules are linked by N—H⋯O, N—H⋯N and C—H⋯N hydrogen bonds, generating sheets lying parallel to (120). |
| format | Online Article Text |
| id | pubmed-4350726 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2015 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-43507262015-04-03 Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide Mohamed, Shaaban K. Knight, Kyle S. Akkurt, Mehmet Hussein, Bahgat R. M. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(9)H(9)ClN(4)OS, the dihedral angle between the acetamide moiety and the pyridine ring is 4.83 (12)°. The O=C—C—Cl torsion angle is 46.4 (3)° and an intramolecular C—H⋯O interaction generates an S(6) ring. In the crystal, molecules are linked by N—H⋯O, N—H⋯N and C—H⋯N hydrogen bonds, generating sheets lying parallel to (120). International Union of Crystallography 2015-02-13 /pmc/articles/PMC4350726/ /pubmed/25844231 http://dx.doi.org/10.1107/S2056989015002431 Text en © Mohamed et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Data Reports Mohamed, Shaaban K. Knight, Kyle S. Akkurt, Mehmet Hussein, Bahgat R. M. Albayati, Mustafa R. Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title | Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title_full | Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title_fullStr | Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title_full_unstemmed | Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title_short | Crystal structure of N-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| title_sort | crystal structure of n-[4-amino-5-cyano-6-(methylsulfanyl)pyridin-2-yl]-2-chloroacetamide |
| topic | Data Reports |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4350726/ https://www.ncbi.nlm.nih.gov/pubmed/25844231 http://dx.doi.org/10.1107/S2056989015002431 |
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