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Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite
Atomic force microscopy, infrared spectroscopy and NMR studied morphological and physicochemical properties of calcium hydroxyapatite powders produced by changing the temperature parameters of synthesis. Features of morphology formation of calcium hydroxyapatite nanoparticles with an annealing tempe...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer US
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4385053/ https://www.ncbi.nlm.nih.gov/pubmed/25852338 http://dx.doi.org/10.1186/s11671-015-0770-1 |
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author | Kurgan, Nataly Karbivskyy, Volodymyr Kasyanenko, Vasyl |
author_facet | Kurgan, Nataly Karbivskyy, Volodymyr Kasyanenko, Vasyl |
author_sort | Kurgan, Nataly |
collection | PubMed |
description | Atomic force microscopy, infrared spectroscopy and NMR studied morphological and physicochemical properties of calcium hydroxyapatite powders produced by changing the temperature parameters of synthesis. Features of morphology formation of calcium hydroxyapatite nanoparticles with an annealing temperature within 200°C to 1,100°C were determined. It is shown that the particle size of the apatite obtained that annealed 700°C is 40 nm corresponding to the particle size of apatite in native bone. The effect of dimension factor on structural parameters of calcium hydroxyapatite is manifested in a more local symmetry of the PO(4)(3−) tetrahedra at nanodispersed calcium hydroxyapatite. |
format | Online Article Text |
id | pubmed-4385053 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | Springer US |
record_format | MEDLINE/PubMed |
spelling | pubmed-43850532015-04-07 Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite Kurgan, Nataly Karbivskyy, Volodymyr Kasyanenko, Vasyl Nanoscale Res Lett Nano Express Atomic force microscopy, infrared spectroscopy and NMR studied morphological and physicochemical properties of calcium hydroxyapatite powders produced by changing the temperature parameters of synthesis. Features of morphology formation of calcium hydroxyapatite nanoparticles with an annealing temperature within 200°C to 1,100°C were determined. It is shown that the particle size of the apatite obtained that annealed 700°C is 40 nm corresponding to the particle size of apatite in native bone. The effect of dimension factor on structural parameters of calcium hydroxyapatite is manifested in a more local symmetry of the PO(4)(3−) tetrahedra at nanodispersed calcium hydroxyapatite. Springer US 2015-02-05 /pmc/articles/PMC4385053/ /pubmed/25852338 http://dx.doi.org/10.1186/s11671-015-0770-1 Text en © Kurgan et al.; licensee Springer. 2015 This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly credited. |
spellingShingle | Nano Express Kurgan, Nataly Karbivskyy, Volodymyr Kasyanenko, Vasyl Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title | Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title_full | Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title_fullStr | Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title_full_unstemmed | Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title_short | Morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
title_sort | morphology and electronic structure of nanoscale powders of calcium hydroxyapatite |
topic | Nano Express |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4385053/ https://www.ncbi.nlm.nih.gov/pubmed/25852338 http://dx.doi.org/10.1186/s11671-015-0770-1 |
work_keys_str_mv | AT kurgannataly morphologyandelectronicstructureofnanoscalepowdersofcalciumhydroxyapatite AT karbivskyyvolodymyr morphologyandelectronicstructureofnanoscalepowdersofcalciumhydroxyapatite AT kasyanenkovasyl morphologyandelectronicstructureofnanoscalepowdersofcalciumhydroxyapatite |