Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine

The asymmetric unit of the title compound, C(23)H(23)N(3), consists of two mol­ecules, A and B, with different conformations. In mol­ecule A, the dihedral angle between the carbazole ring system (r.m.s. deviation = 0.028 Å) and the pyridine ring is 20.28 (9)° and the N—C—C—C torsion angle of the but...

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Autores principales: Zhang, Ping, Bai, Xiang-Yang, Zhang, Ting
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420045/
https://www.ncbi.nlm.nih.gov/pubmed/25995940
http://dx.doi.org/10.1107/S2056989015007975
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author Zhang, Ping
Bai, Xiang-Yang
Zhang, Ting
author_facet Zhang, Ping
Bai, Xiang-Yang
Zhang, Ting
author_sort Zhang, Ping
collection PubMed
description The asymmetric unit of the title compound, C(23)H(23)N(3), consists of two mol­ecules, A and B, with different conformations. In mol­ecule A, the dihedral angle between the carbazole ring system (r.m.s. deviation = 0.028 Å) and the pyridine ring is 20.28 (9)° and the N—C—C—C torsion angle of the butyl side chain is −63.4 (3)°. The equivalent data for mol­ecule B are 0.065 Å, 48.28 (11)° and 61.0 (3)°, respectively. In the crystal, the components are connected by weak N—H⋯N hydrogen bonds, generating [030] C(14) chains of alternating A and B mol­ecules.
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spelling pubmed-44200452015-05-20 Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine Zhang, Ping Bai, Xiang-Yang Zhang, Ting Acta Crystallogr E Crystallogr Commun Data Reports The asymmetric unit of the title compound, C(23)H(23)N(3), consists of two mol­ecules, A and B, with different conformations. In mol­ecule A, the dihedral angle between the carbazole ring system (r.m.s. deviation = 0.028 Å) and the pyridine ring is 20.28 (9)° and the N—C—C—C torsion angle of the butyl side chain is −63.4 (3)°. The equivalent data for mol­ecule B are 0.065 Å, 48.28 (11)° and 61.0 (3)°, respectively. In the crystal, the components are connected by weak N—H⋯N hydrogen bonds, generating [030] C(14) chains of alternating A and B mol­ecules. International Union of Crystallography 2015-04-25 /pmc/articles/PMC4420045/ /pubmed/25995940 http://dx.doi.org/10.1107/S2056989015007975 Text en © Zhang et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Zhang, Ping
Bai, Xiang-Yang
Zhang, Ting
Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title_full Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title_fullStr Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title_full_unstemmed Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title_short Crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
title_sort crystal structure of 9-butyl-6-[2-(pyridin-4-yl)ethen­yl]carbazol-3-amine
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420045/
https://www.ncbi.nlm.nih.gov/pubmed/25995940
http://dx.doi.org/10.1107/S2056989015007975
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