Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate

In the title compound, C(17)H(16)N(2)O(5), the dihedral angles between the central urea [N—C(=O)—N] fragment and its attached benzene rings are 20.20 (14) and 24.24 (13)°; the dihedral angle between the aromatic rings is 42.1 (1)°. The mol­ecular conformation is consolidated by two intra­molecular N...

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Autores principales: Yassine, Hasna, Khouili, Mostafa, El Ammari, Lahcen, Saadi, Mohamed, Ketatni, El Mostafa
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420073/
https://www.ncbi.nlm.nih.gov/pubmed/25995913
http://dx.doi.org/10.1107/S2056989015006465
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author Yassine, Hasna
Khouili, Mostafa
El Ammari, Lahcen
Saadi, Mohamed
Ketatni, El Mostafa
author_facet Yassine, Hasna
Khouili, Mostafa
El Ammari, Lahcen
Saadi, Mohamed
Ketatni, El Mostafa
author_sort Yassine, Hasna
collection PubMed
description In the title compound, C(17)H(16)N(2)O(5), the dihedral angles between the central urea [N—C(=O)—N] fragment and its attached benzene rings are 20.20 (14) and 24.24 (13)°; the dihedral angle between the aromatic rings is 42.1 (1)°. The mol­ecular conformation is consolidated by two intra­molecular N—H⋯O hydrogen bonds, which both generate S(6) rings. In the crystal, inversion dimers linked by pairs of C—H⋯O inter­actions generate R (2) (2)(14) loops. The dimers are linked by further C—H⋯O inter­actions into (011) sheets.
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spelling pubmed-44200732015-05-20 Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate Yassine, Hasna Khouili, Mostafa El Ammari, Lahcen Saadi, Mohamed Ketatni, El Mostafa Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(17)H(16)N(2)O(5), the dihedral angles between the central urea [N—C(=O)—N] fragment and its attached benzene rings are 20.20 (14) and 24.24 (13)°; the dihedral angle between the aromatic rings is 42.1 (1)°. The mol­ecular conformation is consolidated by two intra­molecular N—H⋯O hydrogen bonds, which both generate S(6) rings. In the crystal, inversion dimers linked by pairs of C—H⋯O inter­actions generate R (2) (2)(14) loops. The dimers are linked by further C—H⋯O inter­actions into (011) sheets. International Union of Crystallography 2015-04-09 /pmc/articles/PMC4420073/ /pubmed/25995913 http://dx.doi.org/10.1107/S2056989015006465 Text en © Yassine et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Yassine, Hasna
Khouili, Mostafa
El Ammari, Lahcen
Saadi, Mohamed
Ketatni, El Mostafa
Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title_full Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title_fullStr Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title_full_unstemmed Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title_short Crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
title_sort crystal stucture of methyl 2-({[2-(meth­oxy­carbon­yl)phen­yl]carbamo­yl}amino)­benzoate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420073/
https://www.ncbi.nlm.nih.gov/pubmed/25995913
http://dx.doi.org/10.1107/S2056989015006465
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