Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol

The whole mol­ecule of the title compound, C(22)H(28)Br(2)O(2), is generated by twofold rotation symmetry. The dihedral angle of the biphenyl moiety is 85.05 (11)°. The hy­droxy groups show intra­molecular O—H⋯π inter­actions without any other hydrogen-bond acceptors. In the crystal, there are no ot...

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Autores principales: Obata, Rika, Ohba, Shigeru, Einaga, Yasuaki, Nishiyama, Shigeru
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420096/
https://www.ncbi.nlm.nih.gov/pubmed/25995903
http://dx.doi.org/10.1107/S2056989015006313
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author Obata, Rika
Ohba, Shigeru
Einaga, Yasuaki
Nishiyama, Shigeru
author_facet Obata, Rika
Ohba, Shigeru
Einaga, Yasuaki
Nishiyama, Shigeru
author_sort Obata, Rika
collection PubMed
description The whole mol­ecule of the title compound, C(22)H(28)Br(2)O(2), is generated by twofold rotation symmetry. The dihedral angle of the biphenyl moiety is 85.05 (11)°. The hy­droxy groups show intra­molecular O—H⋯π inter­actions without any other hydrogen-bond acceptors. In the crystal, there are no other significant inter­molecular inter­actions present.
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spelling pubmed-44200962015-05-20 Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol Obata, Rika Ohba, Shigeru Einaga, Yasuaki Nishiyama, Shigeru Acta Crystallogr E Crystallogr Commun Data Reports The whole mol­ecule of the title compound, C(22)H(28)Br(2)O(2), is generated by twofold rotation symmetry. The dihedral angle of the biphenyl moiety is 85.05 (11)°. The hy­droxy groups show intra­molecular O—H⋯π inter­actions without any other hydrogen-bond acceptors. In the crystal, there are no other significant inter­molecular inter­actions present. International Union of Crystallography 2015-04-02 /pmc/articles/PMC4420096/ /pubmed/25995903 http://dx.doi.org/10.1107/S2056989015006313 Text en © Obata et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Obata, Rika
Ohba, Shigeru
Einaga, Yasuaki
Nishiyama, Shigeru
Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title_full Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title_fullStr Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title_full_unstemmed Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title_short Crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
title_sort crystal structure of 5,5′-di­bromo-3,3′-di-tert-butyl-6,6′-di­methyl­biphenyl-2,2′-diol
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420096/
https://www.ncbi.nlm.nih.gov/pubmed/25995903
http://dx.doi.org/10.1107/S2056989015006313
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