Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate

In the title compound, C(18)H(17)ClN(2)O(4), the dihedral angle between the benzofuran ring system [maximum deviation 0.014 (2) Å] and the oxopyradizine ring is 73.33 (8)°. The structure is characterized by disorder of the ethyl group, which is split into two parts, with a major component of 0.57 (3...

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Autores principales: Boukharsa, Youness, El Ammari, Lahcen, Taoufik, Jamal, Saadi, Mohamed, Ansar, M’hammed
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420114/
https://www.ncbi.nlm.nih.gov/pubmed/25995910
http://dx.doi.org/10.1107/S2056989015006301
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author Boukharsa, Youness
El Ammari, Lahcen
Taoufik, Jamal
Saadi, Mohamed
Ansar, M’hammed
author_facet Boukharsa, Youness
El Ammari, Lahcen
Taoufik, Jamal
Saadi, Mohamed
Ansar, M’hammed
author_sort Boukharsa, Youness
collection PubMed
description In the title compound, C(18)H(17)ClN(2)O(4), the dihedral angle between the benzofuran ring system [maximum deviation 0.014 (2) Å] and the oxopyradizine ring is 73.33 (8)°. The structure is characterized by disorder of the ethyl group, which is split into two parts, with a major component of 0.57 (3), and the acetate carbonyl O atom, which is statistically disordered. In the crystal, the molecules are linked by C—H⋯O inter­actions, forming a three-dimensional network.
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spelling pubmed-44201142015-05-20 Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate Boukharsa, Youness El Ammari, Lahcen Taoufik, Jamal Saadi, Mohamed Ansar, M’hammed Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(18)H(17)ClN(2)O(4), the dihedral angle between the benzofuran ring system [maximum deviation 0.014 (2) Å] and the oxopyradizine ring is 73.33 (8)°. The structure is characterized by disorder of the ethyl group, which is split into two parts, with a major component of 0.57 (3), and the acetate carbonyl O atom, which is statistically disordered. In the crystal, the molecules are linked by C—H⋯O inter­actions, forming a three-dimensional network. International Union of Crystallography 2015-04-09 /pmc/articles/PMC4420114/ /pubmed/25995910 http://dx.doi.org/10.1107/S2056989015006301 Text en © Boukharsa et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Boukharsa, Youness
El Ammari, Lahcen
Taoufik, Jamal
Saadi, Mohamed
Ansar, M’hammed
Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title_full Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title_fullStr Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title_full_unstemmed Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title_short Crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
title_sort crystal structure of ethyl 2-{4-[(5-chloro-1-benzo­furan-2-yl)meth­yl]-3-methyl-6-oxo-1,6-di­hydro­pyridazin-1-yl}acetate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420114/
https://www.ncbi.nlm.nih.gov/pubmed/25995910
http://dx.doi.org/10.1107/S2056989015006301
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