Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid

The title compound, C(15)H(17)NO(4)S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb­oxy­lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N—H⋯O hydrogen bond, between the sulfamide N—H g...

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Detalles Bibliográficos
Autores principales: Danish, Muhammad, Tahir, Muhammad Nawaz, Jabeen, Nabila, Raza, Muhammad Asam
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420138/
https://www.ncbi.nlm.nih.gov/pubmed/25995919
http://dx.doi.org/10.1107/S2056989015007057
Descripción
Sumario:The title compound, C(15)H(17)NO(4)S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb­oxy­lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N—H⋯O hydrogen bond, between the sulfamide N—H group and a carb­oxy­lic acid O atom [H⋯O = 2.52 (2) Å], and a C—H⋯O hydrogen bond.

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