Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid

The title compound, C(15)H(17)NO(4)S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb­oxy­lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N—H⋯O hydrogen bond, between the sulfamide N—H g...

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Detalles Bibliográficos
Autores principales: Danish, Muhammad, Tahir, Muhammad Nawaz, Jabeen, Nabila, Raza, Muhammad Asam
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420138/
https://www.ncbi.nlm.nih.gov/pubmed/25995919
http://dx.doi.org/10.1107/S2056989015007057
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author Danish, Muhammad
Tahir, Muhammad Nawaz
Jabeen, Nabila
Raza, Muhammad Asam
author_facet Danish, Muhammad
Tahir, Muhammad Nawaz
Jabeen, Nabila
Raza, Muhammad Asam
author_sort Danish, Muhammad
collection PubMed
description The title compound, C(15)H(17)NO(4)S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb­oxy­lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N—H⋯O hydrogen bond, between the sulfamide N—H group and a carb­oxy­lic acid O atom [H⋯O = 2.52 (2) Å], and a C—H⋯O hydrogen bond.
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spelling pubmed-44201382015-05-20 Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid Danish, Muhammad Tahir, Muhammad Nawaz Jabeen, Nabila Raza, Muhammad Asam Acta Crystallogr E Crystallogr Commun Data Reports The title compound, C(15)H(17)NO(4)S, was synthesized from l-valine and naphthalene-1-sulfonyl chloride. The hydrogen-bonded carb­oxy­lic acid groups form a catemer C(4) motif extending along [100]. The catemer structure is reinforced by a rather long N—H⋯O hydrogen bond, between the sulfamide N—H group and a carb­oxy­lic acid O atom [H⋯O = 2.52 (2) Å], and a C—H⋯O hydrogen bond. International Union of Crystallography 2015-04-15 /pmc/articles/PMC4420138/ /pubmed/25995919 http://dx.doi.org/10.1107/S2056989015007057 Text en © Danish et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Danish, Muhammad
Tahir, Muhammad Nawaz
Jabeen, Nabila
Raza, Muhammad Asam
Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title_full Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title_fullStr Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title_full_unstemmed Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title_short Crystal structure of (2S)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
title_sort crystal structure of (2s)-3-methyl-2-[(naphthalen-1-ylsulfon­yl)amino]­butanoic acid
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420138/
https://www.ncbi.nlm.nih.gov/pubmed/25995919
http://dx.doi.org/10.1107/S2056989015007057
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