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Chemicals from Agave sisalana Biomass: Isolation and Identification

Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liqui...

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Autores principales: Santos, Jener David Gonçalves, Vieira, Ivo Jose Curcino, Braz-Filho, Raimundo, Branco, Alexsandro
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4425107/
https://www.ncbi.nlm.nih.gov/pubmed/25903149
http://dx.doi.org/10.3390/ijms16048761
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author Santos, Jener David Gonçalves
Vieira, Ivo Jose Curcino
Braz-Filho, Raimundo
Branco, Alexsandro
author_facet Santos, Jener David Gonçalves
Vieira, Ivo Jose Curcino
Braz-Filho, Raimundo
Branco, Alexsandro
author_sort Santos, Jener David Gonçalves
collection PubMed
description Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liquid-liquid extraction, crystallization, SiO(2) and Sephadex LH 20 column chromatography) to obtain pectin, mannitol, succinic acid, kaempferol and a mixture of saponins as raw chemicals from sisal biomass. The structural identification of these compounds was performed though spectrometric methods, such as Infrared (IR), Ultraviolet (UV), Mass spectrometry (MS) and Nuclear magnetic resonance (NMR). All the sisal chemicals found in this work are used by both the chemical and pharmaceutical industries as excipients or active principles in products.
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spelling pubmed-44251072015-05-20 Chemicals from Agave sisalana Biomass: Isolation and Identification Santos, Jener David Gonçalves Vieira, Ivo Jose Curcino Braz-Filho, Raimundo Branco, Alexsandro Int J Mol Sci Article Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liquid-liquid extraction, crystallization, SiO(2) and Sephadex LH 20 column chromatography) to obtain pectin, mannitol, succinic acid, kaempferol and a mixture of saponins as raw chemicals from sisal biomass. The structural identification of these compounds was performed though spectrometric methods, such as Infrared (IR), Ultraviolet (UV), Mass spectrometry (MS) and Nuclear magnetic resonance (NMR). All the sisal chemicals found in this work are used by both the chemical and pharmaceutical industries as excipients or active principles in products. MDPI 2015-04-20 /pmc/articles/PMC4425107/ /pubmed/25903149 http://dx.doi.org/10.3390/ijms16048761 Text en © 2015 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Santos, Jener David Gonçalves
Vieira, Ivo Jose Curcino
Braz-Filho, Raimundo
Branco, Alexsandro
Chemicals from Agave sisalana Biomass: Isolation and Identification
title Chemicals from Agave sisalana Biomass: Isolation and Identification
title_full Chemicals from Agave sisalana Biomass: Isolation and Identification
title_fullStr Chemicals from Agave sisalana Biomass: Isolation and Identification
title_full_unstemmed Chemicals from Agave sisalana Biomass: Isolation and Identification
title_short Chemicals from Agave sisalana Biomass: Isolation and Identification
title_sort chemicals from agave sisalana biomass: isolation and identification
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4425107/
https://www.ncbi.nlm.nih.gov/pubmed/25903149
http://dx.doi.org/10.3390/ijms16048761
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