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Chemicals from Agave sisalana Biomass: Isolation and Identification
Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liqui...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4425107/ https://www.ncbi.nlm.nih.gov/pubmed/25903149 http://dx.doi.org/10.3390/ijms16048761 |
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author | Santos, Jener David Gonçalves Vieira, Ivo Jose Curcino Braz-Filho, Raimundo Branco, Alexsandro |
author_facet | Santos, Jener David Gonçalves Vieira, Ivo Jose Curcino Braz-Filho, Raimundo Branco, Alexsandro |
author_sort | Santos, Jener David Gonçalves |
collection | PubMed |
description | Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liquid-liquid extraction, crystallization, SiO(2) and Sephadex LH 20 column chromatography) to obtain pectin, mannitol, succinic acid, kaempferol and a mixture of saponins as raw chemicals from sisal biomass. The structural identification of these compounds was performed though spectrometric methods, such as Infrared (IR), Ultraviolet (UV), Mass spectrometry (MS) and Nuclear magnetic resonance (NMR). All the sisal chemicals found in this work are used by both the chemical and pharmaceutical industries as excipients or active principles in products. |
format | Online Article Text |
id | pubmed-4425107 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-44251072015-05-20 Chemicals from Agave sisalana Biomass: Isolation and Identification Santos, Jener David Gonçalves Vieira, Ivo Jose Curcino Braz-Filho, Raimundo Branco, Alexsandro Int J Mol Sci Article Agave sisalana (sisal) is known worldwide as a source of hard fibers, and Brazil is the largest producer of sisal. Nonetheless, the process of removing the fibers of the sisal leaf generates 95% waste. In this study, we applied chemical sequential steps (hydrothermal extraction, precipitation, liquid-liquid extraction, crystallization, SiO(2) and Sephadex LH 20 column chromatography) to obtain pectin, mannitol, succinic acid, kaempferol and a mixture of saponins as raw chemicals from sisal biomass. The structural identification of these compounds was performed though spectrometric methods, such as Infrared (IR), Ultraviolet (UV), Mass spectrometry (MS) and Nuclear magnetic resonance (NMR). All the sisal chemicals found in this work are used by both the chemical and pharmaceutical industries as excipients or active principles in products. MDPI 2015-04-20 /pmc/articles/PMC4425107/ /pubmed/25903149 http://dx.doi.org/10.3390/ijms16048761 Text en © 2015 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Santos, Jener David Gonçalves Vieira, Ivo Jose Curcino Braz-Filho, Raimundo Branco, Alexsandro Chemicals from Agave sisalana Biomass: Isolation and Identification |
title | Chemicals from Agave sisalana Biomass: Isolation and Identification |
title_full | Chemicals from Agave sisalana Biomass: Isolation and Identification |
title_fullStr | Chemicals from Agave sisalana Biomass: Isolation and Identification |
title_full_unstemmed | Chemicals from Agave sisalana Biomass: Isolation and Identification |
title_short | Chemicals from Agave sisalana Biomass: Isolation and Identification |
title_sort | chemicals from agave sisalana biomass: isolation and identification |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4425107/ https://www.ncbi.nlm.nih.gov/pubmed/25903149 http://dx.doi.org/10.3390/ijms16048761 |
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