Crystal structure of 4-meth­oxy-N-[(pyrrolidin-1-yl)carbo­thio­yl]benzamide

In the title compound, C(13)H(16)N(2)O(2)S, the pyrrolidine ring has a twisted conformation on the central –CH(2)–CH(2)– bond. Its mean plane is inclined to the 4-meth­oxy­benzoyl ring by 72.79 (15)°. In the crystal, mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds to the same O-atom acceptor...

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Detalles Bibliográficos
Autores principales: Suhud, Khairi, Heng, Lee Yook, Hasbullah, Siti Aishah, Ahmad, Musa, Kassim, Mohammad B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4438823/
https://www.ncbi.nlm.nih.gov/pubmed/26029426
http://dx.doi.org/10.1107/S2056989015003813
Descripción
Sumario:In the title compound, C(13)H(16)N(2)O(2)S, the pyrrolidine ring has a twisted conformation on the central –CH(2)–CH(2)– bond. Its mean plane is inclined to the 4-meth­oxy­benzoyl ring by 72.79 (15)°. In the crystal, mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds to the same O-atom acceptor, forming chains along [001]. The chains are linked via slipped parallel π–π inter­actions [inter-centroid distance = 3.7578 (13) Å], forming undulating slabs parallel to (100).

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