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Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin

In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using...

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Detalles Bibliográficos
Autores principales: Jiang, B., Zhu, C. C., Huang, Y. D.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Public Library of Science 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4465346/
https://www.ncbi.nlm.nih.gov/pubmed/26061002
http://dx.doi.org/10.1371/journal.pone.0127735
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author Jiang, B.
Zhu, C. C.
Huang, Y. D.
author_facet Jiang, B.
Zhu, C. C.
Huang, Y. D.
author_sort Jiang, B.
collection PubMed
description In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using hexadecyl trimethyl ammonium bromide as the intercalating agent. Then, functional sericite was incorporated into methylphenyl-silicone by terminal hydroxyl. The structure and dispersive performance of the hybrid polymers was charactered by analytical instruments. Scanning electron microscopy and Transmission electron microscope, Laser scanning confocal microscope and X-ray diffraction analysis showed that functional sericite was dispersed homogeneously in methylphenyl-silicone resin matrix. X-ray photoelectron spectroscopy analysis showed that the absorption peaks of the Si-OH band of methylphenyl-silicone resin were decreased and the Si-O-Si band was increased. This change evidently showed a significant role to enhance the reaction degree of the functional sericite in methylphenyl-silicone resin.
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spelling pubmed-44653462015-06-25 Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin Jiang, B. Zhu, C. C. Huang, Y. D. PLoS One Research Article In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using hexadecyl trimethyl ammonium bromide as the intercalating agent. Then, functional sericite was incorporated into methylphenyl-silicone by terminal hydroxyl. The structure and dispersive performance of the hybrid polymers was charactered by analytical instruments. Scanning electron microscopy and Transmission electron microscope, Laser scanning confocal microscope and X-ray diffraction analysis showed that functional sericite was dispersed homogeneously in methylphenyl-silicone resin matrix. X-ray photoelectron spectroscopy analysis showed that the absorption peaks of the Si-OH band of methylphenyl-silicone resin were decreased and the Si-O-Si band was increased. This change evidently showed a significant role to enhance the reaction degree of the functional sericite in methylphenyl-silicone resin. Public Library of Science 2015-06-10 /pmc/articles/PMC4465346/ /pubmed/26061002 http://dx.doi.org/10.1371/journal.pone.0127735 Text en © 2015 Jiang et al http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are properly credited.
spellingShingle Research Article
Jiang, B.
Zhu, C. C.
Huang, Y. D.
Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title_full Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title_fullStr Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title_full_unstemmed Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title_short Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
title_sort research of the dispersity of the functional sericite/methylphenyl- silicone resin
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4465346/
https://www.ncbi.nlm.nih.gov/pubmed/26061002
http://dx.doi.org/10.1371/journal.pone.0127735
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