Cargando…
Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin
In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using...
Autores principales: | , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Public Library of Science
2015
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4465346/ https://www.ncbi.nlm.nih.gov/pubmed/26061002 http://dx.doi.org/10.1371/journal.pone.0127735 |
_version_ | 1782376087311876096 |
---|---|
author | Jiang, B. Zhu, C. C. Huang, Y. D. |
author_facet | Jiang, B. Zhu, C. C. Huang, Y. D. |
author_sort | Jiang, B. |
collection | PubMed |
description | In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using hexadecyl trimethyl ammonium bromide as the intercalating agent. Then, functional sericite was incorporated into methylphenyl-silicone by terminal hydroxyl. The structure and dispersive performance of the hybrid polymers was charactered by analytical instruments. Scanning electron microscopy and Transmission electron microscope, Laser scanning confocal microscope and X-ray diffraction analysis showed that functional sericite was dispersed homogeneously in methylphenyl-silicone resin matrix. X-ray photoelectron spectroscopy analysis showed that the absorption peaks of the Si-OH band of methylphenyl-silicone resin were decreased and the Si-O-Si band was increased. This change evidently showed a significant role to enhance the reaction degree of the functional sericite in methylphenyl-silicone resin. |
format | Online Article Text |
id | pubmed-4465346 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | Public Library of Science |
record_format | MEDLINE/PubMed |
spelling | pubmed-44653462015-06-25 Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin Jiang, B. Zhu, C. C. Huang, Y. D. PLoS One Research Article In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using hexadecyl trimethyl ammonium bromide as the intercalating agent. Then, functional sericite was incorporated into methylphenyl-silicone by terminal hydroxyl. The structure and dispersive performance of the hybrid polymers was charactered by analytical instruments. Scanning electron microscopy and Transmission electron microscope, Laser scanning confocal microscope and X-ray diffraction analysis showed that functional sericite was dispersed homogeneously in methylphenyl-silicone resin matrix. X-ray photoelectron spectroscopy analysis showed that the absorption peaks of the Si-OH band of methylphenyl-silicone resin were decreased and the Si-O-Si band was increased. This change evidently showed a significant role to enhance the reaction degree of the functional sericite in methylphenyl-silicone resin. Public Library of Science 2015-06-10 /pmc/articles/PMC4465346/ /pubmed/26061002 http://dx.doi.org/10.1371/journal.pone.0127735 Text en © 2015 Jiang et al http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are properly credited. |
spellingShingle | Research Article Jiang, B. Zhu, C. C. Huang, Y. D. Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title | Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title_full | Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title_fullStr | Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title_full_unstemmed | Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title_short | Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
title_sort | research of the dispersity of the functional sericite/methylphenyl- silicone resin |
topic | Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4465346/ https://www.ncbi.nlm.nih.gov/pubmed/26061002 http://dx.doi.org/10.1371/journal.pone.0127735 |
work_keys_str_mv | AT jiangb researchofthedispersityofthefunctionalsericitemethylphenylsiliconeresin AT zhucc researchofthedispersityofthefunctionalsericitemethylphenylsiliconeresin AT huangyd researchofthedispersityofthefunctionalsericitemethylphenylsiliconeresin |