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A Convenient Synthetic Protocol to 1,2-Bis(dialkylphosphino)ethanes

1,2-Bis(dialkylphosphino)ethanes are readily prepared from the parent phosphine oxides, via a novel sodium aluminium hydride/sodium hydride reduction protocol of intermediate chlorophosphonium chlorides. This approach is amenable to multi-gram syntheses, utilises readily available and inexpensive re...

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Detalles Bibliográficos
Autores principales:	Doyle, Laurence R, Heath, Alex, Low, Choon Heng, Ashley, Andrew E
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	WILEY-VCH Verlag 2014
Materias:	Updates
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4498470/ https://www.ncbi.nlm.nih.gov/pubmed/26190960 http://dx.doi.org/10.1002/adsc.201300787

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