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Ultra-stable sub-meV monochromator for hard X-rays
A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in (151)Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4542453/ https://www.ncbi.nlm.nih.gov/pubmed/26289266 http://dx.doi.org/10.1107/S1600577515012230 |
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author | Toellner, T. S. Collins, J. Goetze, K. Hu, M. Y. Preissner, C. Trakhtenberg, E. Yan, L. |
author_facet | Toellner, T. S. Collins, J. Goetze, K. Hu, M. Y. Preissner, C. Trakhtenberg, E. Yan, L. |
author_sort | Toellner, T. S. |
collection | PubMed |
description | A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in (151)Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017 meV r.m.s. per day, or a 100-fold improvement over other meV-monochromators, and can tolerate higher X-ray power loads than room-temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high-speed Doppler shifting. The design of the monochromator along with its performance and impact on transmitted beam properties are presented. |
format | Online Article Text |
id | pubmed-4542453 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-45424532015-08-24 Ultra-stable sub-meV monochromator for hard X-rays Toellner, T. S. Collins, J. Goetze, K. Hu, M. Y. Preissner, C. Trakhtenberg, E. Yan, L. J Synchrotron Radiat Research Papers A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in (151)Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017 meV r.m.s. per day, or a 100-fold improvement over other meV-monochromators, and can tolerate higher X-ray power loads than room-temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high-speed Doppler shifting. The design of the monochromator along with its performance and impact on transmitted beam properties are presented. International Union of Crystallography 2015-07-17 /pmc/articles/PMC4542453/ /pubmed/26289266 http://dx.doi.org/10.1107/S1600577515012230 Text en © T. S. Toellner et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Toellner, T. S. Collins, J. Goetze, K. Hu, M. Y. Preissner, C. Trakhtenberg, E. Yan, L. Ultra-stable sub-meV monochromator for hard X-rays |
title | Ultra-stable sub-meV monochromator for hard X-rays |
title_full | Ultra-stable sub-meV monochromator for hard X-rays |
title_fullStr | Ultra-stable sub-meV monochromator for hard X-rays |
title_full_unstemmed | Ultra-stable sub-meV monochromator for hard X-rays |
title_short | Ultra-stable sub-meV monochromator for hard X-rays |
title_sort | ultra-stable sub-mev monochromator for hard x-rays |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4542453/ https://www.ncbi.nlm.nih.gov/pubmed/26289266 http://dx.doi.org/10.1107/S1600577515012230 |
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