Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide

In the title compound, C(16)H(17)N(3)OS, a benzoyl thio­urea derivative, the planes of the pyridine and benzene rings are inclined to one another by 66.54 (9)°. There is an intra­molecular N—H⋯O hydrogen bond present forming an S(6) ring motif. In the crystal, mol­ecules are linked via pairs of N—H⋯...

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Autores principales: Ameram, Nadiah, Adam, Farook
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555406/
https://www.ncbi.nlm.nih.gov/pubmed/26396877
http://dx.doi.org/10.1107/S2056989015013559
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author Ameram, Nadiah
Adam, Farook
author_facet Ameram, Nadiah
Adam, Farook
author_sort Ameram, Nadiah
collection PubMed
description In the title compound, C(16)H(17)N(3)OS, a benzoyl thio­urea derivative, the planes of the pyridine and benzene rings are inclined to one another by 66.54 (9)°. There is an intra­molecular N—H⋯O hydrogen bond present forming an S(6) ring motif. In the crystal, mol­ecules are linked via pairs of N—H⋯N hydrogen bonds, forming inversion dimers, which are reinforced by pairs of C—H⋯S hydrogen bonds. The dimers are linked via C—H⋯π inter­actions, forming ribbons along [010].
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spelling pubmed-45554062015-09-22 Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide Ameram, Nadiah Adam, Farook Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(16)H(17)N(3)OS, a benzoyl thio­urea derivative, the planes of the pyridine and benzene rings are inclined to one another by 66.54 (9)°. There is an intra­molecular N—H⋯O hydrogen bond present forming an S(6) ring motif. In the crystal, mol­ecules are linked via pairs of N—H⋯N hydrogen bonds, forming inversion dimers, which are reinforced by pairs of C—H⋯S hydrogen bonds. The dimers are linked via C—H⋯π inter­actions, forming ribbons along [010]. International Union of Crystallography 2015-08-06 /pmc/articles/PMC4555406/ /pubmed/26396877 http://dx.doi.org/10.1107/S2056989015013559 Text en © Ameram and Adam 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Ameram, Nadiah
Adam, Farook
Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title_full Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title_fullStr Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title_full_unstemmed Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title_short Crystal structure of 2-methyl-N-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
title_sort crystal structure of 2-methyl-n-{[2-(pyri­din-2-yl)eth­yl]carbamo­thio­yl}benzamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555406/
https://www.ncbi.nlm.nih.gov/pubmed/26396877
http://dx.doi.org/10.1107/S2056989015013559
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