A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate

The title compound, C(15)H(17)NO(4), containing two mol­ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol­ecule in the asymmetric unit. Both mol­ecules in the title c...

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Detalles Bibliográficos
Autores principales: Guo, Ailing, Zhang, Shurong, Wang, Kun, Zhu, Ruitao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555412/
https://www.ncbi.nlm.nih.gov/pubmed/26396905
http://dx.doi.org/10.1107/S205698901501539X
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author Guo, Ailing
Zhang, Shurong
Wang, Kun
Zhu, Ruitao
author_facet Guo, Ailing
Zhang, Shurong
Wang, Kun
Zhu, Ruitao
author_sort Guo, Ailing
collection PubMed
description The title compound, C(15)H(17)NO(4), containing two mol­ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol­ecule in the asymmetric unit. Both mol­ecules in the title compound are in the trans form. In the crystal, N—H⋯O and O—H⋯O hydrogen bonds connect mol­ecules, forming a two-dimensional network parallel to (001).
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spelling pubmed-45554122015-09-22 A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate Guo, Ailing Zhang, Shurong Wang, Kun Zhu, Ruitao Acta Crystallogr E Crystallogr Commun Data Reports The title compound, C(15)H(17)NO(4), containing two mol­ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol­ecule in the asymmetric unit. Both mol­ecules in the title compound are in the trans form. In the crystal, N—H⋯O and O—H⋯O hydrogen bonds connect mol­ecules, forming a two-dimensional network parallel to (001). International Union of Crystallography 2015-08-26 /pmc/articles/PMC4555412/ /pubmed/26396905 http://dx.doi.org/10.1107/S205698901501539X Text en © Guo et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Guo, Ailing
Zhang, Shurong
Wang, Kun
Zhu, Ruitao
A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title_full A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title_fullStr A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title_full_unstemmed A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title_short A new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
title_sort new polymorph of 1-({[1,3-dihy­droxy-2-(hy­droxy­meth­yl)propan-2-yl]iminio}meth­yl)naphthalen-2-olate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555412/
https://www.ncbi.nlm.nih.gov/pubmed/26396905
http://dx.doi.org/10.1107/S205698901501539X
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