Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone

In the title compound, C(7)H(13)NOS(2), the thio­morpholine ring adopts a chair conformation and the bond-angle sum at the N atom is 360°. The dihedral angle between the amide group and the thio­morpholine ring (all atoms) is 36.48 (12)°. In the crystal, C—H⋯O and C—H⋯S hydrogen bonds link adjacent...

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Autores principales: Kang, Gihaeng, Kim, Jineun, Kwon, Eunjin, Kim, Tae Ho
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555416/
https://www.ncbi.nlm.nih.gov/pubmed/26396901
http://dx.doi.org/10.1107/S2056989015015418
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author Kang, Gihaeng
Kim, Jineun
Kwon, Eunjin
Kim, Tae Ho
author_facet Kang, Gihaeng
Kim, Jineun
Kwon, Eunjin
Kim, Tae Ho
author_sort Kang, Gihaeng
collection PubMed
description In the title compound, C(7)H(13)NOS(2), the thio­morpholine ring adopts a chair conformation and the bond-angle sum at the N atom is 360°. The dihedral angle between the amide group and the thio­morpholine ring (all atoms) is 36.48 (12)°. In the crystal, C—H⋯O and C—H⋯S hydrogen bonds link adjacent mol­ecules, forming two-dimensional networks extending parellel to the (011) plane.
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spelling pubmed-45554162015-09-22 Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone Kang, Gihaeng Kim, Jineun Kwon, Eunjin Kim, Tae Ho Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(7)H(13)NOS(2), the thio­morpholine ring adopts a chair conformation and the bond-angle sum at the N atom is 360°. The dihedral angle between the amide group and the thio­morpholine ring (all atoms) is 36.48 (12)°. In the crystal, C—H⋯O and C—H⋯S hydrogen bonds link adjacent mol­ecules, forming two-dimensional networks extending parellel to the (011) plane. International Union of Crystallography 2015-08-22 /pmc/articles/PMC4555416/ /pubmed/26396901 http://dx.doi.org/10.1107/S2056989015015418 Text en © Kang et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Kang, Gihaeng
Kim, Jineun
Kwon, Eunjin
Kim, Tae Ho
Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title_full Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title_fullStr Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title_full_unstemmed Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title_short Crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
title_sort crystal structure of 2-methyl­sulfanyl-1-(thio­morpholin-4-yl)­ethanone
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555416/
https://www.ncbi.nlm.nih.gov/pubmed/26396901
http://dx.doi.org/10.1107/S2056989015015418
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