Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)

In the title compound, C(11)H(12)N(2)O(2)·C(4)H(4)O(4)·H(2)O, the l-tryp­to­phan mol­ecule crystallized as a zwitterion, together with a neutral fumaric acid mol­ecule and a water solvent mol­ecule. In the crystal, the three components are linked by a series of N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds,...

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Detalles Bibliográficos
Autores principales: Caroline, M. Lydia, Kumaresan, S., Aravindan, P. G., Mohamed, M. Peer, Mani, G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555439/
https://www.ncbi.nlm.nih.gov/pubmed/26396891
http://dx.doi.org/10.1107/S205698901501484X
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author Caroline, M. Lydia
Kumaresan, S.
Aravindan, P. G.
Mohamed, M. Peer
Mani, G.
author_facet Caroline, M. Lydia
Kumaresan, S.
Aravindan, P. G.
Mohamed, M. Peer
Mani, G.
author_sort Caroline, M. Lydia
collection PubMed
description In the title compound, C(11)H(12)N(2)O(2)·C(4)H(4)O(4)·H(2)O, the l-tryp­to­phan mol­ecule crystallized as a zwitterion, together with a neutral fumaric acid mol­ecule and a water solvent mol­ecule. In the crystal, the three components are linked by a series of N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds, forming slabs lying parallel to (001). The slabs are connected by O—H⋯O hydrogen bonds, involving inversion-related fumaric acid groups, leading to the formation of a three-dimensional structure.
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spelling pubmed-45554392015-09-22 Crystal structure of l-tryptophan–fumaric acid–water (1/1/1) Caroline, M. Lydia Kumaresan, S. Aravindan, P. G. Mohamed, M. Peer Mani, G. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(11)H(12)N(2)O(2)·C(4)H(4)O(4)·H(2)O, the l-tryp­to­phan mol­ecule crystallized as a zwitterion, together with a neutral fumaric acid mol­ecule and a water solvent mol­ecule. In the crystal, the three components are linked by a series of N—H⋯O, O—H⋯O and C—H⋯O hydrogen bonds, forming slabs lying parallel to (001). The slabs are connected by O—H⋯O hydrogen bonds, involving inversion-related fumaric acid groups, leading to the formation of a three-dimensional structure. International Union of Crystallography 2015-08-15 /pmc/articles/PMC4555439/ /pubmed/26396891 http://dx.doi.org/10.1107/S205698901501484X Text en © Caroline et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Caroline, M. Lydia
Kumaresan, S.
Aravindan, P. G.
Mohamed, M. Peer
Mani, G.
Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title_full Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title_fullStr Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title_full_unstemmed Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title_short Crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
title_sort crystal structure of l-tryptophan–fumaric acid–water (1/1/1)
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555439/
https://www.ncbi.nlm.nih.gov/pubmed/26396891
http://dx.doi.org/10.1107/S205698901501484X
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