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Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct

The crystal structure of the title salt adduct, 2C(6)H(14)N(+)·C(4)H(4)O(4) (2−)·C(4)H(6)O(4), consists of two cyclo­hexyl­ammonium cations, one succcinate dianion and one neutral succinic acid mol­ecule. Succinate dianions and succinic acid mol­ecules are self-assembled head-to-tail through O—H⋯O h...

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Autores principales: Sarr, Modou, Diasse-Sarr, Aminata, Diop, Libasse, Plasseraud, Laurent, Cattey, Hélène
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571351/
https://www.ncbi.nlm.nih.gov/pubmed/26396750
http://dx.doi.org/10.1107/S2056989015012621
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author Sarr, Modou
Diasse-Sarr, Aminata
Diop, Libasse
Plasseraud, Laurent
Cattey, Hélène
author_facet Sarr, Modou
Diasse-Sarr, Aminata
Diop, Libasse
Plasseraud, Laurent
Cattey, Hélène
author_sort Sarr, Modou
collection PubMed
description The crystal structure of the title salt adduct, 2C(6)H(14)N(+)·C(4)H(4)O(4) (2−)·C(4)H(6)O(4), consists of two cyclo­hexyl­ammonium cations, one succcinate dianion and one neutral succinic acid mol­ecule. Succinate dianions and succinic acid mol­ecules are self-assembled head-to-tail through O—H⋯O hydrogen bonds and adopt a syn–syn configuration, leading to a strand-like arrangement along [101]. The cyclo­hexyl­ammonium cations have a chair conformation and act as multidentate hydrogen-bond donors linking adjacent strands through inter­molecular N—H⋯O inter­actions to both the succinate and the succinic acid components. This results in two-dimensional supra­molecular layered structures lying parallel to (010).
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spelling pubmed-45713512015-09-22 Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct Sarr, Modou Diasse-Sarr, Aminata Diop, Libasse Plasseraud, Laurent Cattey, Hélène Acta Crystallogr E Crystallogr Commun Research Communications The crystal structure of the title salt adduct, 2C(6)H(14)N(+)·C(4)H(4)O(4) (2−)·C(4)H(6)O(4), consists of two cyclo­hexyl­ammonium cations, one succcinate dianion and one neutral succinic acid mol­ecule. Succinate dianions and succinic acid mol­ecules are self-assembled head-to-tail through O—H⋯O hydrogen bonds and adopt a syn–syn configuration, leading to a strand-like arrangement along [101]. The cyclo­hexyl­ammonium cations have a chair conformation and act as multidentate hydrogen-bond donors linking adjacent strands through inter­molecular N—H⋯O inter­actions to both the succinate and the succinic acid components. This results in two-dimensional supra­molecular layered structures lying parallel to (010). International Union of Crystallography 2015-07-08 /pmc/articles/PMC4571351/ /pubmed/26396750 http://dx.doi.org/10.1107/S2056989015012621 Text en © Sarr et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Sarr, Modou
Diasse-Sarr, Aminata
Diop, Libasse
Plasseraud, Laurent
Cattey, Hélène
Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title_full Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title_fullStr Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title_full_unstemmed Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title_short Crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
title_sort crystal structure of the bis­(cyclo­hexyl­ammonium) succinate succinic acid salt adduct
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571351/
https://www.ncbi.nlm.nih.gov/pubmed/26396750
http://dx.doi.org/10.1107/S2056989015012621
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