Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate

In the title compound, C(12)H(10)ClNO(3), the asymmetric unit comprises two independent mol­ecules, and the dihedral angle between the least-square planes of the quinoline ring systems of these mol­ecules is 73.30 (5)°. In the crystal, N—H⋯O hydrogen bonds between the independent mol­ecules lead to...

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Autores principales: Ishikawa, Yoshinobu, Yoshida, Nanako
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571399/
https://www.ncbi.nlm.nih.gov/pubmed/26396799
http://dx.doi.org/10.1107/S2056989015013171
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author Ishikawa, Yoshinobu
Yoshida, Nanako
author_facet Ishikawa, Yoshinobu
Yoshida, Nanako
author_sort Ishikawa, Yoshinobu
collection PubMed
description In the title compound, C(12)H(10)ClNO(3), the asymmetric unit comprises two independent mol­ecules, and the dihedral angle between the least-square planes of the quinoline ring systems of these mol­ecules is 73.30 (5)°. In the crystal, N—H⋯O hydrogen bonds between the independent mol­ecules lead to supra­molecular layers parallel to (-1-10); both N—H H atoms are bifurcated.
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spelling pubmed-45713992015-09-22 Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate Ishikawa, Yoshinobu Yoshida, Nanako Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(12)H(10)ClNO(3), the asymmetric unit comprises two independent mol­ecules, and the dihedral angle between the least-square planes of the quinoline ring systems of these mol­ecules is 73.30 (5)°. In the crystal, N—H⋯O hydrogen bonds between the independent mol­ecules lead to supra­molecular layers parallel to (-1-10); both N—H H atoms are bifurcated. International Union of Crystallography 2015-07-15 /pmc/articles/PMC4571399/ /pubmed/26396799 http://dx.doi.org/10.1107/S2056989015013171 Text en © Ishikawa and Yoshida 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Ishikawa, Yoshinobu
Yoshida, Nanako
Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title_full Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title_fullStr Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title_full_unstemmed Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title_short Crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
title_sort crystal structure of ethyl 8-chloro-4-oxo-1,4-di­hydro­quinoline-3-carboxyl­ate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571399/
https://www.ncbi.nlm.nih.gov/pubmed/26396799
http://dx.doi.org/10.1107/S2056989015013171
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