Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one

The title compound, C(13)H(13)Cl(2)NO, has a 3-(propan-2-yl­idene)indolin-2-one core with a Cl atom and a chloro­ethyl substituent attached to the aromatic ring. Two atoms of the aromatic ring and the chloro­ethyl substituent atoms are disordered over two sets of sites with a refined occupancy ratio...

Descripción completa

Detalles Bibliográficos
Autores principales: Roopashree, K. R., Meti, Gangadhar Y., Kamble, Ravindra R., Devarajegowda, H. C.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571414/
https://www.ncbi.nlm.nih.gov/pubmed/26396814
http://dx.doi.org/10.1107/S2056989015012268
_version_ 1782390336545357824
author Roopashree, K. R.
Meti, Gangadhar Y.
Kamble, Ravindra R.
Devarajegowda, H. C.
author_facet Roopashree, K. R.
Meti, Gangadhar Y.
Kamble, Ravindra R.
Devarajegowda, H. C.
author_sort Roopashree, K. R.
collection PubMed
description The title compound, C(13)H(13)Cl(2)NO, has a 3-(propan-2-yl­idene)indolin-2-one core with a Cl atom and a chloro­ethyl substituent attached to the aromatic ring. Two atoms of the aromatic ring and the chloro­ethyl substituent atoms are disordered over two sets of sites with a refined occupancy ratio of 0.826 (3):0.174 (3). In the crystal, mol­ecules are linked by pairs of N—H⋯O hydrogen bonds, forming inversion dimers with an R (2) (2)(8) ring motif.
format Online
Article
Text
id pubmed-4571414
institution National Center for Biotechnology Information
language English
publishDate 2015
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-45714142015-09-22 Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one Roopashree, K. R. Meti, Gangadhar Y. Kamble, Ravindra R. Devarajegowda, H. C. Acta Crystallogr E Crystallogr Commun Data Reports The title compound, C(13)H(13)Cl(2)NO, has a 3-(propan-2-yl­idene)indolin-2-one core with a Cl atom and a chloro­ethyl substituent attached to the aromatic ring. Two atoms of the aromatic ring and the chloro­ethyl substituent atoms are disordered over two sets of sites with a refined occupancy ratio of 0.826 (3):0.174 (3). In the crystal, mol­ecules are linked by pairs of N—H⋯O hydrogen bonds, forming inversion dimers with an R (2) (2)(8) ring motif. International Union of Crystallography 2015-07-22 /pmc/articles/PMC4571414/ /pubmed/26396814 http://dx.doi.org/10.1107/S2056989015012268 Text en © Roopashree et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Roopashree, K. R.
Meti, Gangadhar Y.
Kamble, Ravindra R.
Devarajegowda, H. C.
Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title_full Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title_fullStr Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title_full_unstemmed Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title_short Crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
title_sort crystal structure of 6-chloro-5-(2-chloro­eth­yl)-3-(propan-2-yl­idene)indolin-2-one
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4571414/
https://www.ncbi.nlm.nih.gov/pubmed/26396814
http://dx.doi.org/10.1107/S2056989015012268
work_keys_str_mv AT roopashreekr crystalstructureof6chloro52chloroethyl3propan2ylideneindolin2one
AT metigangadhary crystalstructureof6chloro52chloroethyl3propan2ylideneindolin2one
AT kambleravindrar crystalstructureof6chloro52chloroethyl3propan2ylideneindolin2one
AT devarajegowdahc crystalstructureof6chloro52chloroethyl3propan2ylideneindolin2one

Ejemplares similares