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A simple method for the determination of qPlus sensor spring constants
qPlus sensors are widely used to measure forces at the atomic scale, however, confidence in these measurements is limited by inconsistent reports of the spring constant of the sensor and complications from finite tip heights. Here we combine a numerical investigation of the force reconstruction with...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Beilstein-Institut
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4578344/ https://www.ncbi.nlm.nih.gov/pubmed/26425425 http://dx.doi.org/10.3762/bjnano.6.177 |
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author | Melcher, John Stirling, Julian Shaw, Gordon A |
author_facet | Melcher, John Stirling, Julian Shaw, Gordon A |
author_sort | Melcher, John |
collection | PubMed |
description | qPlus sensors are widely used to measure forces at the atomic scale, however, confidence in these measurements is limited by inconsistent reports of the spring constant of the sensor and complications from finite tip heights. Here we combine a numerical investigation of the force reconstruction with an experimental characterization of the flexural mechanics of the qPlus sensor. Numerical studies reveal significant errors in reconstructed force for tip heights exceeding 400 μm or one sixth of the cantilever length. Experimental results with a calibrated nanoindenter reveal excellent agreement with an Euler–Bernoulli beam model for the sensor. Prior to the attachment of a tip, measured spring constants of 1902 ± 29 N/m are found to be in agreement with theoretical predictions for the geometry and material properties of the sensor once a peaked ridge in the beam cross section is included. We further develop a correction necessary to adjust the spring constant for the size and placement of the tip. |
format | Online Article Text |
id | pubmed-4578344 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | Beilstein-Institut |
record_format | MEDLINE/PubMed |
spelling | pubmed-45783442015-09-30 A simple method for the determination of qPlus sensor spring constants Melcher, John Stirling, Julian Shaw, Gordon A Beilstein J Nanotechnol Full Research Paper qPlus sensors are widely used to measure forces at the atomic scale, however, confidence in these measurements is limited by inconsistent reports of the spring constant of the sensor and complications from finite tip heights. Here we combine a numerical investigation of the force reconstruction with an experimental characterization of the flexural mechanics of the qPlus sensor. Numerical studies reveal significant errors in reconstructed force for tip heights exceeding 400 μm or one sixth of the cantilever length. Experimental results with a calibrated nanoindenter reveal excellent agreement with an Euler–Bernoulli beam model for the sensor. Prior to the attachment of a tip, measured spring constants of 1902 ± 29 N/m are found to be in agreement with theoretical predictions for the geometry and material properties of the sensor once a peaked ridge in the beam cross section is included. We further develop a correction necessary to adjust the spring constant for the size and placement of the tip. Beilstein-Institut 2015-08-14 /pmc/articles/PMC4578344/ /pubmed/26425425 http://dx.doi.org/10.3762/bjnano.6.177 Text en Copyright © 2015, Melcher et al. https://creativecommons.org/licenses/by/2.0https://www.beilstein-journals.org/bjnano/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/2.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited. The license is subject to the Beilstein Journal of Nanotechnology terms and conditions: (https://www.beilstein-journals.org/bjnano/terms) |
spellingShingle | Full Research Paper Melcher, John Stirling, Julian Shaw, Gordon A A simple method for the determination of qPlus sensor spring constants |
title | A simple method for the determination of qPlus sensor spring constants |
title_full | A simple method for the determination of qPlus sensor spring constants |
title_fullStr | A simple method for the determination of qPlus sensor spring constants |
title_full_unstemmed | A simple method for the determination of qPlus sensor spring constants |
title_short | A simple method for the determination of qPlus sensor spring constants |
title_sort | simple method for the determination of qplus sensor spring constants |
topic | Full Research Paper |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4578344/ https://www.ncbi.nlm.nih.gov/pubmed/26425425 http://dx.doi.org/10.3762/bjnano.6.177 |
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