Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)

Slow co-crystallization of a solution of benzene-1,3,5-tri­carb­oxy­lic acid with a large excess of 4-hy­droxy­pyridine produces an inter­penetrating, three-dimensional, hydrogen-bonded framework consisting of three 4-pyridone and one benzene-1,3,5-tri­carb­oxy­lic acid mol­ecules, C(9)H(6)O(6)·3C(5...

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Detalles Bibliográficos
Autores principales: Staun, Selena L., Oliver, Allen G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4644998/
https://www.ncbi.nlm.nih.gov/pubmed/26594492
http://dx.doi.org/10.1107/S2056989015017867
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author Staun, Selena L.
Oliver, Allen G.
author_facet Staun, Selena L.
Oliver, Allen G.
author_sort Staun, Selena L.
collection PubMed
description Slow co-crystallization of a solution of benzene-1,3,5-tri­carb­oxy­lic acid with a large excess of 4-hy­droxy­pyridine produces an inter­penetrating, three-dimensional, hydrogen-bonded framework consisting of three 4-pyridone and one benzene-1,3,5-tri­carb­oxy­lic acid mol­ecules, C(9)H(6)O(6)·3C(5)H(5)NO. This structure represents an ortho­rhom­bic polymorph of the previously reported C-centered, monoclinic structure [Campos-Gaxiola et al. (2014 ▸). Acta Cryst. E70, o453–o454].
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spelling pubmed-46449982015-11-20 Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3) Staun, Selena L. Oliver, Allen G. Acta Crystallogr E Crystallogr Commun Research Communications Slow co-crystallization of a solution of benzene-1,3,5-tri­carb­oxy­lic acid with a large excess of 4-hy­droxy­pyridine produces an inter­penetrating, three-dimensional, hydrogen-bonded framework consisting of three 4-pyridone and one benzene-1,3,5-tri­carb­oxy­lic acid mol­ecules, C(9)H(6)O(6)·3C(5)H(5)NO. This structure represents an ortho­rhom­bic polymorph of the previously reported C-centered, monoclinic structure [Campos-Gaxiola et al. (2014 ▸). Acta Cryst. E70, o453–o454]. International Union of Crystallography 2015-10-03 /pmc/articles/PMC4644998/ /pubmed/26594492 http://dx.doi.org/10.1107/S2056989015017867 Text en © Staun and Oliver 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Staun, Selena L.
Oliver, Allen G.
Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title_full Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title_fullStr Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title_full_unstemmed Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title_short Crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
title_sort crystal structure of benzene-1,3,5-tri­carb­oxy­lic acid–4-pyridone (1/3)
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4644998/
https://www.ncbi.nlm.nih.gov/pubmed/26594492
http://dx.doi.org/10.1107/S2056989015017867
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