Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide

In the title compound, C(10)H(7)FN(2)OS, the mean plane of the central amide fragment (r.m.s. deviation = 0.048 Å) makes dihedral angles of 35.28 (8) and 10.14 (12)° with those of the fluoro­benzene and thia­zole rings, respectively. The thia­zole S and amide O atoms lie to the same side of the mol­...

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Autores principales: Moreno-Fuquen, Rodolfo, Castillo, Juan C., Becerra, Diana, Camargo, Hernando, Henao, José A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645012/
https://www.ncbi.nlm.nih.gov/pubmed/26594578
http://dx.doi.org/10.1107/S2056989015019192
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author Moreno-Fuquen, Rodolfo
Castillo, Juan C.
Becerra, Diana
Camargo, Hernando
Henao, José A.
author_facet Moreno-Fuquen, Rodolfo
Castillo, Juan C.
Becerra, Diana
Camargo, Hernando
Henao, José A.
author_sort Moreno-Fuquen, Rodolfo
collection PubMed
description In the title compound, C(10)H(7)FN(2)OS, the mean plane of the central amide fragment (r.m.s. deviation = 0.048 Å) makes dihedral angles of 35.28 (8) and 10.14 (12)° with those of the fluoro­benzene and thia­zole rings, respectively. The thia­zole S and amide O atoms lie to the same side of the mol­ecule. In the crystal, pairs of N—H⋯N hydrogen bonds connect the mol­ecules into inversion dimers with R (2) (2)(8) motifs, and weak C—H⋯O inter­actions connect the mol­ecules into C(6) [001] chains. Together, the N—H⋯N and C—H⋯O hydrogen bonds generate (100) sheets.
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spelling pubmed-46450122015-11-20 Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide Moreno-Fuquen, Rodolfo Castillo, Juan C. Becerra, Diana Camargo, Hernando Henao, José A. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(10)H(7)FN(2)OS, the mean plane of the central amide fragment (r.m.s. deviation = 0.048 Å) makes dihedral angles of 35.28 (8) and 10.14 (12)° with those of the fluoro­benzene and thia­zole rings, respectively. The thia­zole S and amide O atoms lie to the same side of the mol­ecule. In the crystal, pairs of N—H⋯N hydrogen bonds connect the mol­ecules into inversion dimers with R (2) (2)(8) motifs, and weak C—H⋯O inter­actions connect the mol­ecules into C(6) [001] chains. Together, the N—H⋯N and C—H⋯O hydrogen bonds generate (100) sheets. International Union of Crystallography 2015-10-24 /pmc/articles/PMC4645012/ /pubmed/26594578 http://dx.doi.org/10.1107/S2056989015019192 Text en © Moreno-Fuquen et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Moreno-Fuquen, Rodolfo
Castillo, Juan C.
Becerra, Diana
Camargo, Hernando
Henao, José A.
Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title_full Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title_fullStr Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title_full_unstemmed Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title_short Crystal structure of 2-fluoro-N-(1,3-thia­zol-2-yl)benzamide
title_sort crystal structure of 2-fluoro-n-(1,3-thia­zol-2-yl)benzamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645012/
https://www.ncbi.nlm.nih.gov/pubmed/26594578
http://dx.doi.org/10.1107/S2056989015019192
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