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Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate

In the title compound, C(21)H(19)N(3)O(3)S, the 5,6,7,8-tetra­hydro­pyridine ring adopts a half-chair conformation. The fused-thieno[2,3-d]pyrimidine ring system is essentially planar (r.m.s. deviation = 0.001 Å) and forms a dihedral angle of 2.66 (6)° with the attached phenyl ring. The three-dimens...

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Autores principales: Akkurt, Mehmet, Smolenski, Victoria A., Mohamed, Shaaban K., Jasinski, Jerry P., Ahmed, Essam K, Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645036/
https://www.ncbi.nlm.nih.gov/pubmed/26594553
http://dx.doi.org/10.1107/S2056989015018447
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author Akkurt, Mehmet
Smolenski, Victoria A.
Mohamed, Shaaban K.
Jasinski, Jerry P.
Ahmed, Essam K
Albayati, Mustafa R.
author_facet Akkurt, Mehmet
Smolenski, Victoria A.
Mohamed, Shaaban K.
Jasinski, Jerry P.
Ahmed, Essam K
Albayati, Mustafa R.
author_sort Akkurt, Mehmet
collection PubMed
description In the title compound, C(21)H(19)N(3)O(3)S, the 5,6,7,8-tetra­hydro­pyridine ring adopts a half-chair conformation. The fused-thieno[2,3-d]pyrimidine ring system is essentially planar (r.m.s. deviation = 0.001 Å) and forms a dihedral angle of 2.66 (6)° with the attached phenyl ring. The three-dimensional crystal packing is stabilized by C—H⋯O and C—H⋯N hydrogen bonds and C—H⋯π inter­actions.
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spelling pubmed-46450362015-11-20 Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate Akkurt, Mehmet Smolenski, Victoria A. Mohamed, Shaaban K. Jasinski, Jerry P. Ahmed, Essam K Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(21)H(19)N(3)O(3)S, the 5,6,7,8-tetra­hydro­pyridine ring adopts a half-chair conformation. The fused-thieno[2,3-d]pyrimidine ring system is essentially planar (r.m.s. deviation = 0.001 Å) and forms a dihedral angle of 2.66 (6)° with the attached phenyl ring. The three-dimensional crystal packing is stabilized by C—H⋯O and C—H⋯N hydrogen bonds and C—H⋯π inter­actions. International Union of Crystallography 2015-10-10 /pmc/articles/PMC4645036/ /pubmed/26594553 http://dx.doi.org/10.1107/S2056989015018447 Text en © Akkurt et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Akkurt, Mehmet
Smolenski, Victoria A.
Mohamed, Shaaban K.
Jasinski, Jerry P.
Ahmed, Essam K
Albayati, Mustafa R.
Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title_full Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title_fullStr Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title_full_unstemmed Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title_short Crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
title_sort crystal structure of ethyl 2-phenyl-4-(prop-2-yn-1-yl­oxy)-5,6,7,8-tetra­hydro­pyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7-carboxyl­ate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645036/
https://www.ncbi.nlm.nih.gov/pubmed/26594553
http://dx.doi.org/10.1107/S2056989015018447
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