Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide

In the title piperidine derivative, C(21)H(22)Cl(2)N(2)O, the piperidine ring adopts a chair conformation. The chloro­phenyl rings are oriented at an angle of 45.59 (14)° with respect to each other. In the crystal, mol­ecules are linked via N—H⋯O hydrogen bonds, forming C(4) chains along [100]. The...

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Detalles Bibliográficos
Autores principales: Priya, K., Saravanan, K., Selvanayagam, S., Kabilan, S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645048/
https://www.ncbi.nlm.nih.gov/pubmed/26594551
http://dx.doi.org/10.1107/S2056989015018666
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author Priya, K.
Saravanan, K.
Selvanayagam, S.
Kabilan, S.
author_facet Priya, K.
Saravanan, K.
Selvanayagam, S.
Kabilan, S.
author_sort Priya, K.
collection PubMed
description In the title piperidine derivative, C(21)H(22)Cl(2)N(2)O, the piperidine ring adopts a chair conformation. The chloro­phenyl rings are oriented at an angle of 45.59 (14)° with respect to each other. In the crystal, mol­ecules are linked via N—H⋯O hydrogen bonds, forming C(4) chains along [100]. The chains are linked by C—H⋯O hydrogen bonds, forming sheets parallel to the ab plane. Within the sheets, there are N—H⋯π inter­actions present. The crystal studied was refined as an inversion twin.
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spelling pubmed-46450482015-11-20 Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide Priya, K. Saravanan, K. Selvanayagam, S. Kabilan, S. Acta Crystallogr E Crystallogr Commun Data Reports In the title piperidine derivative, C(21)H(22)Cl(2)N(2)O, the piperidine ring adopts a chair conformation. The chloro­phenyl rings are oriented at an angle of 45.59 (14)° with respect to each other. In the crystal, mol­ecules are linked via N—H⋯O hydrogen bonds, forming C(4) chains along [100]. The chains are linked by C—H⋯O hydrogen bonds, forming sheets parallel to the ab plane. Within the sheets, there are N—H⋯π inter­actions present. The crystal studied was refined as an inversion twin. International Union of Crystallography 2015-10-10 /pmc/articles/PMC4645048/ /pubmed/26594551 http://dx.doi.org/10.1107/S2056989015018666 Text en © Priya et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Priya, K.
Saravanan, K.
Selvanayagam, S.
Kabilan, S.
Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title_full Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title_fullStr Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title_full_unstemmed Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title_short Crystal structure of 2-[4(E)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
title_sort crystal structure of 2-[4(e)-2,6-bis­(4-chloro­phen­yl)-3-ethyl­piperidin-4-yl­idene]acetamide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645048/
https://www.ncbi.nlm.nih.gov/pubmed/26594551
http://dx.doi.org/10.1107/S2056989015018666
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AT saravanank crystalstructureof24e26bis4chlorophenyl3ethylpiperidin4ylideneacetamide
AT selvanayagams crystalstructureof24e26bis4chlorophenyl3ethylpiperidin4ylideneacetamide
AT kabilans crystalstructureof24e26bis4chlorophenyl3ethylpiperidin4ylideneacetamide

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