The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate

The complete mol­ecule of the title compound, C(30)H(29)N(3)O(5)S(2), is generated by a crystallographic twofold axis: the O atom and NH group attached to the central benzene ring are statistically disordered. The dihedral angle between the naphthalene ring system and the central benzene ring is 52....

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Autores principales: Chainok, Kittipong, Duangthongyou, Tanwawan, Tuntulani, Thawatchai, Chuenka, Apinya, Wannalerse, Boontana
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4647440/
https://www.ncbi.nlm.nih.gov/pubmed/26594442
http://dx.doi.org/10.1107/S2056989015016199
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author Chainok, Kittipong
Duangthongyou, Tanwawan
Tuntulani, Thawatchai
Chuenka, Apinya
Wannalerse, Boontana
author_facet Chainok, Kittipong
Duangthongyou, Tanwawan
Tuntulani, Thawatchai
Chuenka, Apinya
Wannalerse, Boontana
author_sort Chainok, Kittipong
collection PubMed
description The complete mol­ecule of the title compound, C(30)H(29)N(3)O(5)S(2), is generated by a crystallographic twofold axis: the O atom and NH group attached to the central benzene ring are statistically disordered. The dihedral angle between the naphthalene ring system and the central benzene ring is 52.99 (6)°, while the pendant naphthalene ring systems subtend a dihedral angle of 68.17 (4)°. An intra­molecular C—H⋯O hydrogen bond closes an S(6) ring. In the crystal, the mol­ecules are linked by weak C—H⋯O hydrogen bonds.
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spelling pubmed-46474402015-11-20 The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate Chainok, Kittipong Duangthongyou, Tanwawan Tuntulani, Thawatchai Chuenka, Apinya Wannalerse, Boontana Acta Crystallogr E Crystallogr Commun Data Reports The complete mol­ecule of the title compound, C(30)H(29)N(3)O(5)S(2), is generated by a crystallographic twofold axis: the O atom and NH group attached to the central benzene ring are statistically disordered. The dihedral angle between the naphthalene ring system and the central benzene ring is 52.99 (6)°, while the pendant naphthalene ring systems subtend a dihedral angle of 68.17 (4)°. An intra­molecular C—H⋯O hydrogen bond closes an S(6) ring. In the crystal, the mol­ecules are linked by weak C—H⋯O hydrogen bonds. International Union of Crystallography 2015-09-12 /pmc/articles/PMC4647440/ /pubmed/26594442 http://dx.doi.org/10.1107/S2056989015016199 Text en © Chainok et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Chainok, Kittipong
Duangthongyou, Tanwawan
Tuntulani, Thawatchai
Chuenka, Apinya
Wannalerse, Boontana
The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title_full The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title_fullStr The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title_full_unstemmed The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title_short The crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
title_sort crystal structure of 2-[5-(di­methyl­amino)­naphthalene-1-sulfonamido]­phenyl 5-(di­methyl­amino)­naphthalene-1-sulfonate
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4647440/
https://www.ncbi.nlm.nih.gov/pubmed/26594442
http://dx.doi.org/10.1107/S2056989015016199
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