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Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2

Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc...

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Detalles Bibliográficos
Autores principales: Radulescu, Aurel, Székely, Noémi Kinga, Polachowski, Stephan, Leyendecker, Marko, Amann, Matthias, Buitenhuis, Johan, Drochner, Matthias, Engels, Ralf, Hanslik, Romuald, Kemmerling, Günter, Lindner, Peter, Papagiannopoulos, Aristeidis, Pipich, Vitaliy, Willner, Lutz, Frielinghaus, Henrich, Richter, Dieter
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4665661/
https://www.ncbi.nlm.nih.gov/pubmed/26664343
http://dx.doi.org/10.1107/S1600576715019019
Descripción
Sumario:Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes.