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Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2
Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc...
Autores principales: | , , , , , , , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4665661/ https://www.ncbi.nlm.nih.gov/pubmed/26664343 http://dx.doi.org/10.1107/S1600576715019019 |
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author | Radulescu, Aurel Székely, Noémi Kinga Polachowski, Stephan Leyendecker, Marko Amann, Matthias Buitenhuis, Johan Drochner, Matthias Engels, Ralf Hanslik, Romuald Kemmerling, Günter Lindner, Peter Papagiannopoulos, Aristeidis Pipich, Vitaliy Willner, Lutz Frielinghaus, Henrich Richter, Dieter |
author_facet | Radulescu, Aurel Székely, Noémi Kinga Polachowski, Stephan Leyendecker, Marko Amann, Matthias Buitenhuis, Johan Drochner, Matthias Engels, Ralf Hanslik, Romuald Kemmerling, Günter Lindner, Peter Papagiannopoulos, Aristeidis Pipich, Vitaliy Willner, Lutz Frielinghaus, Henrich Richter, Dieter |
author_sort | Radulescu, Aurel |
collection | PubMed |
description | Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes. |
format | Online Article Text |
id | pubmed-4665661 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-46656612015-12-10 Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 Radulescu, Aurel Székely, Noémi Kinga Polachowski, Stephan Leyendecker, Marko Amann, Matthias Buitenhuis, Johan Drochner, Matthias Engels, Ralf Hanslik, Romuald Kemmerling, Günter Lindner, Peter Papagiannopoulos, Aristeidis Pipich, Vitaliy Willner, Lutz Frielinghaus, Henrich Richter, Dieter J Appl Crystallogr Research Papers Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes. International Union of Crystallography 2015-11-19 /pmc/articles/PMC4665661/ /pubmed/26664343 http://dx.doi.org/10.1107/S1600576715019019 Text en © Aurel Radulescu et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Radulescu, Aurel Székely, Noémi Kinga Polachowski, Stephan Leyendecker, Marko Amann, Matthias Buitenhuis, Johan Drochner, Matthias Engels, Ralf Hanslik, Romuald Kemmerling, Günter Lindner, Peter Papagiannopoulos, Aristeidis Pipich, Vitaliy Willner, Lutz Frielinghaus, Henrich Richter, Dieter Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title | Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title_full | Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title_fullStr | Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title_full_unstemmed | Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title_short | Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2 |
title_sort | tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer kws-2 |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4665661/ https://www.ncbi.nlm.nih.gov/pubmed/26664343 http://dx.doi.org/10.1107/S1600576715019019 |
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