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Development of Sensitive and Specific Analysis of Vildagliptin in Pharmaceutical Formulation by Gas Chromatography-Mass Spectrometry

A sensitive and selective gas chromatography-mass spectrometry (GC-MS) method was developed and fully validated for the determination of vildagliptin (VIL) in pharmaceutical formulation. Prior to GC-MS analysis, VIL was efficiently derivatized with MSTFA/NH(4)I/β-mercaptoethanol at 60°C for 30 min....

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Detalles Bibliográficos
Autor principal:	Uçaktürk, Ebru
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Hindawi Publishing Corporation 2015
Materias:	Research Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4670650/ https://www.ncbi.nlm.nih.gov/pubmed/26682085 http://dx.doi.org/10.1155/2015/707414

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