Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea

In the title compound, C(9)H(15)N(3)S, the cyclo­pentyl ring adopts an envelope conformation with one of the methyl­ene C atoms as the flap. The thio­semicarbazide fragment is almost planar (r.m.s. deviation = 0.038 Å) and a short intra­molecular N—H⋯N contact occurs. In the crystal, mol­ecules are...

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Autores principales: Mohamed, Shaaban K., Mague, Joel T., Akkurt, Mehmet, Hassan, Alaa A., Abdel-Aziz, Ahmed T., Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719883/
https://www.ncbi.nlm.nih.gov/pubmed/26870530
http://dx.doi.org/10.1107/S2056989015021003
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author Mohamed, Shaaban K.
Mague, Joel T.
Akkurt, Mehmet
Hassan, Alaa A.
Abdel-Aziz, Ahmed T.
Albayati, Mustafa R.
author_facet Mohamed, Shaaban K.
Mague, Joel T.
Akkurt, Mehmet
Hassan, Alaa A.
Abdel-Aziz, Ahmed T.
Albayati, Mustafa R.
author_sort Mohamed, Shaaban K.
collection PubMed
description In the title compound, C(9)H(15)N(3)S, the cyclo­pentyl ring adopts an envelope conformation with one of the methyl­ene C atoms as the flap. The thio­semicarbazide fragment is almost planar (r.m.s. deviation = 0.038 Å) and a short intra­molecular N—H⋯N contact occurs. In the crystal, mol­ecules are linked into helical (4(1) symmetry) chains propagating in [001] by N—H⋯N and N—H⋯S hydrogen bonds. A very weak C—H⋯S inter­action is also observed.
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spelling pubmed-47198832016-02-11 Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea Mohamed, Shaaban K. Mague, Joel T. Akkurt, Mehmet Hassan, Alaa A. Abdel-Aziz, Ahmed T. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(9)H(15)N(3)S, the cyclo­pentyl ring adopts an envelope conformation with one of the methyl­ene C atoms as the flap. The thio­semicarbazide fragment is almost planar (r.m.s. deviation = 0.038 Å) and a short intra­molecular N—H⋯N contact occurs. In the crystal, mol­ecules are linked into helical (4(1) symmetry) chains propagating in [001] by N—H⋯N and N—H⋯S hydrogen bonds. A very weak C—H⋯S inter­action is also observed. International Union of Crystallography 2015-11-11 /pmc/articles/PMC4719883/ /pubmed/26870530 http://dx.doi.org/10.1107/S2056989015021003 Text en © Mohamed et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Mohamed, Shaaban K.
Mague, Joel T.
Akkurt, Mehmet
Hassan, Alaa A.
Abdel-Aziz, Ahmed T.
Albayati, Mustafa R.
Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title_full Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title_fullStr Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title_full_unstemmed Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title_short Crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
title_sort crystal structure of 1-(cyclo­pentyl­idene­amino)-3-(prop-2-en-1-yl)thio­urea
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719883/
https://www.ncbi.nlm.nih.gov/pubmed/26870530
http://dx.doi.org/10.1107/S2056989015021003
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