Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide

In the title compound, C(22)H(18)ClN(3)O, the carbazole ring system is essentially planar (r.m.s deviation = 0.003 Å), and makes a dihedral angle of 9.01 (8)° with the plane of the chloro­phenyl ring. In the crystal, neighbouring mol­ecules are linked into centrosymmetric R (2) (2)(8) dimers by pair...

Descripción completa

Detalles Bibliográficos
Autores principales: Akkurt, Mehmet, Jasinski, Jerry P., Mohamed, Shaaban K., El-Emary, Talaat I., Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719890/
https://www.ncbi.nlm.nih.gov/pubmed/26870537
http://dx.doi.org/10.1107/S2056989015020770
_version_ 1782410996340490240
author Akkurt, Mehmet
Jasinski, Jerry P.
Mohamed, Shaaban K.
El-Emary, Talaat I.
Albayati, Mustafa R.
author_facet Akkurt, Mehmet
Jasinski, Jerry P.
Mohamed, Shaaban K.
El-Emary, Talaat I.
Albayati, Mustafa R.
author_sort Akkurt, Mehmet
collection PubMed
description In the title compound, C(22)H(18)ClN(3)O, the carbazole ring system is essentially planar (r.m.s deviation = 0.003 Å), and makes a dihedral angle of 9.01 (8)° with the plane of the chloro­phenyl ring. In the crystal, neighbouring mol­ecules are linked into centrosymmetric R (2) (2)(8) dimers by pairs of N—H⋯O inter­actions and into a three-dimensional network by C—H⋯π inter­actions. The dimers are arranged into layers parallel to (010).
format Online
Article
Text
id pubmed-4719890
institution National Center for Biotechnology Information
language English
publishDate 2015
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-47198902016-02-11 Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide Akkurt, Mehmet Jasinski, Jerry P. Mohamed, Shaaban K. El-Emary, Talaat I. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(22)H(18)ClN(3)O, the carbazole ring system is essentially planar (r.m.s deviation = 0.003 Å), and makes a dihedral angle of 9.01 (8)° with the plane of the chloro­phenyl ring. In the crystal, neighbouring mol­ecules are linked into centrosymmetric R (2) (2)(8) dimers by pairs of N—H⋯O inter­actions and into a three-dimensional network by C—H⋯π inter­actions. The dimers are arranged into layers parallel to (010). International Union of Crystallography 2015-11-14 /pmc/articles/PMC4719890/ /pubmed/26870537 http://dx.doi.org/10.1107/S2056989015020770 Text en © Akkurt et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Akkurt, Mehmet
Jasinski, Jerry P.
Mohamed, Shaaban K.
El-Emary, Talaat I.
Albayati, Mustafa R.
Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title_full Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title_fullStr Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title_full_unstemmed Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title_short Crystal structure of 3-(9H-carbazol-9-yl)-N′-[(E)-4-chloro­benzyl­idene]propano­hydrazide
title_sort crystal structure of 3-(9h-carbazol-9-yl)-n′-[(e)-4-chloro­benzyl­idene]propano­hydrazide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719890/
https://www.ncbi.nlm.nih.gov/pubmed/26870537
http://dx.doi.org/10.1107/S2056989015020770
work_keys_str_mv AT akkurtmehmet crystalstructureof39hcarbazol9ylne4chlorobenzylidenepropanohydrazide
AT jasinskijerryp crystalstructureof39hcarbazol9ylne4chlorobenzylidenepropanohydrazide
AT mohamedshaabank crystalstructureof39hcarbazol9ylne4chlorobenzylidenepropanohydrazide
AT elemarytalaati crystalstructureof39hcarbazol9ylne4chlorobenzylidenepropanohydrazide
AT albayatimustafar crystalstructureof39hcarbazol9ylne4chlorobenzylidenepropanohydrazide

Ejemplares similares