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Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol

In the mol­ecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-di­hydro­benzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and th...

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Detalles Bibliográficos
Autores principales: Adam, Farook, Arafath, Md. Azharul, Rosenani, A. Haque, Razali, Mohd. R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719928/
https://www.ncbi.nlm.nih.gov/pubmed/26870556
http://dx.doi.org/10.1107/S2056989015021180
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author Adam, Farook
Arafath, Md. Azharul
Rosenani, A. Haque
Razali, Mohd. R.
author_facet Adam, Farook
Arafath, Md. Azharul
Rosenani, A. Haque
Razali, Mohd. R.
author_sort Adam, Farook
collection PubMed
description In the mol­ecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-di­hydro­benzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and the benzene ring of the quinazoline group are 14.28 (5) and 4.7 (3)° for the major and minor disorder components, respectively. An intra­molecular O—H⋯O hydrogen bond is present. In the crystal, mol­ecules are linked by O—H⋯N hydrogen bonds, forming chains running parallel to [10-1].
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spelling pubmed-47199282016-02-11 Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol Adam, Farook Arafath, Md. Azharul Rosenani, A. Haque Razali, Mohd. R. Acta Crystallogr E Crystallogr Commun Data Reports In the mol­ecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-di­hydro­benzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and the benzene ring of the quinazoline group are 14.28 (5) and 4.7 (3)° for the major and minor disorder components, respectively. An intra­molecular O—H⋯O hydrogen bond is present. In the crystal, mol­ecules are linked by O—H⋯N hydrogen bonds, forming chains running parallel to [10-1]. International Union of Crystallography 2015-11-21 /pmc/articles/PMC4719928/ /pubmed/26870556 http://dx.doi.org/10.1107/S2056989015021180 Text en © Adam et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Adam, Farook
Arafath, Md. Azharul
Rosenani, A. Haque
Razali, Mohd. R.
Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title_full Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title_fullStr Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title_full_unstemmed Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title_short Crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
title_sort crystal structure of 5-(5,6-di­hydro­benzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-meth­oxy­phenol
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719928/
https://www.ncbi.nlm.nih.gov/pubmed/26870556
http://dx.doi.org/10.1107/S2056989015021180
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