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Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol
In the molecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-dihydrobenzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and th...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719928/ https://www.ncbi.nlm.nih.gov/pubmed/26870556 http://dx.doi.org/10.1107/S2056989015021180 |
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author | Adam, Farook Arafath, Md. Azharul Rosenani, A. Haque Razali, Mohd. R. |
author_facet | Adam, Farook Arafath, Md. Azharul Rosenani, A. Haque Razali, Mohd. R. |
author_sort | Adam, Farook |
collection | PubMed |
description | In the molecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-dihydrobenzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and the benzene ring of the quinazoline group are 14.28 (5) and 4.7 (3)° for the major and minor disorder components, respectively. An intramolecular O—H⋯O hydrogen bond is present. In the crystal, molecules are linked by O—H⋯N hydrogen bonds, forming chains running parallel to [10-1]. |
format | Online Article Text |
id | pubmed-4719928 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2015 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-47199282016-02-11 Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol Adam, Farook Arafath, Md. Azharul Rosenani, A. Haque Razali, Mohd. R. Acta Crystallogr E Crystallogr Commun Data Reports In the molecule of the title compound, C(21)H(17)N(3)O(2), the 5,6-dihydrobenzimidazo[1,2-c]quinazoline moiety is disordered over two orientations about a pseudo-mirror plane, with a refined occupancy ratio of 0.863 (2):0.137 (2). The dihedral angles formed by the benzimidazole ring system and the benzene ring of the quinazoline group are 14.28 (5) and 4.7 (3)° for the major and minor disorder components, respectively. An intramolecular O—H⋯O hydrogen bond is present. In the crystal, molecules are linked by O—H⋯N hydrogen bonds, forming chains running parallel to [10-1]. International Union of Crystallography 2015-11-21 /pmc/articles/PMC4719928/ /pubmed/26870556 http://dx.doi.org/10.1107/S2056989015021180 Text en © Adam et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Data Reports Adam, Farook Arafath, Md. Azharul Rosenani, A. Haque Razali, Mohd. R. Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title | Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title_full | Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title_fullStr | Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title_full_unstemmed | Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title_short | Crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
title_sort | crystal structure of 5-(5,6-dihydrobenzo[4,5]imidazo[1,2-c]quinazolin-6-yl)-2-methoxyphenol |
topic | Data Reports |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719928/ https://www.ncbi.nlm.nih.gov/pubmed/26870556 http://dx.doi.org/10.1107/S2056989015021180 |
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