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Crystal structure of 3-benzyl-1-[(1,2,3,4-tetrahydronaphthalen-1-ylidene)amino]thiourea
In the title compound, C(18)H(19)N(3)S, the dihedral angle between the planes of the benzene rings is 58.63 (8)°. The six-membered ring bonded to the thiosemicarbazide group (r.m.s. deviation = 0.038 Å) adopts a sofa conformation, with one of the methylene-group C atoms as the flap. A short intra...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719930/ https://www.ncbi.nlm.nih.gov/pubmed/26870558 http://dx.doi.org/10.1107/S2056989015021064 |
Sumario: | In the title compound, C(18)H(19)N(3)S, the dihedral angle between the planes of the benzene rings is 58.63 (8)°. The six-membered ring bonded to the thiosemicarbazide group (r.m.s. deviation = 0.038 Å) adopts a sofa conformation, with one of the methylene-group C atoms as the flap. A short intramolecular N—H⋯N contact is observed. In the crystal, molecules are linked by weak N—H⋯S interactions to generate C(4) chains propagating in the [010] direction, with adjacent molecules related by glide symmetry. |
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