Cargando…
Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea
In the title compound, C(14)H(17)N(3)S, the dihedral angle between the planes of the benzene ring and the thiosemicarbazone group (r.m.s. deviation = 0.031 Å) is 8.45 (4)°. A short intramolcular N—H⋯N contact is seen. In the crystal, weak N—H⋯S hydrogen bonds connect the molecules into C(4) chain...
| Autores principales: | , , , , , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2015
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719931/ https://www.ncbi.nlm.nih.gov/pubmed/26870559 http://dx.doi.org/10.1107/S2056989015021076 |
| _version_ | 1782411005571104768 |
|---|---|
| author | Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Hassan, Alaa A Abdel-Aziz, Ahmed T. Albayati, Mustafa R. |
| author_facet | Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Hassan, Alaa A Abdel-Aziz, Ahmed T. Albayati, Mustafa R. |
| author_sort | Mague, Joel T. |
| collection | PubMed |
| description | In the title compound, C(14)H(17)N(3)S, the dihedral angle between the planes of the benzene ring and the thiosemicarbazone group (r.m.s. deviation = 0.031 Å) is 8.45 (4)°. A short intramolcular N—H⋯N contact is seen. In the crystal, weak N—H⋯S hydrogen bonds connect the molecules into C(4) chains propagating in the [010] direction, with adjacent molecules in the chain related by 2(1) screw-axis symmetry. |
| format | Online Article Text |
| id | pubmed-4719931 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2015 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-47199312016-02-11 Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Hassan, Alaa A Abdel-Aziz, Ahmed T. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(14)H(17)N(3)S, the dihedral angle between the planes of the benzene ring and the thiosemicarbazone group (r.m.s. deviation = 0.031 Å) is 8.45 (4)°. A short intramolcular N—H⋯N contact is seen. In the crystal, weak N—H⋯S hydrogen bonds connect the molecules into C(4) chains propagating in the [010] direction, with adjacent molecules in the chain related by 2(1) screw-axis symmetry. International Union of Crystallography 2015-11-21 /pmc/articles/PMC4719931/ /pubmed/26870559 http://dx.doi.org/10.1107/S2056989015021076 Text en © Mague et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Data Reports Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Hassan, Alaa A Abdel-Aziz, Ahmed T. Albayati, Mustafa R. Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title | Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title_full | Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title_fullStr | Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title_full_unstemmed | Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title_short | Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| title_sort | crystal structure of 3-(prop-2-en-1-yl)-1-{[(1e)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea |
| topic | Data Reports |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719931/ https://www.ncbi.nlm.nih.gov/pubmed/26870559 http://dx.doi.org/10.1107/S2056989015021076 |
| work_keys_str_mv | AT maguejoelt crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea AT mohamedshaabank crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea AT akkurtmehmet crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea AT hassanalaaa crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea AT abdelazizahmedt crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea AT albayatimustafar crystalstructureof3prop2en1yl11e1234tetrahydronaphthalen1ylideneaminothiourea |