Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide

In the title compound, C(16)H(12)N(2)O(3), the 2H-chromene moiety is essentially planar, with an r.m.s. deviation of the nine constituent atoms from the mean plane of 0.0093 Å, and makes a dihedral angle of 76.84 (3)° with the pendant phenyl ring. An intra­molecular N—H⋯O hydrogen bond helps to dete...

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Autores principales: Mague, Joel T., Mohamed, Shaaban K., Akkurt, Mehmet, Younes, Sabry H. H., Albayati, Mustafa R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719947/
https://www.ncbi.nlm.nih.gov/pubmed/26870466
http://dx.doi.org/10.1107/S2056989015022495
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author Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Younes, Sabry H. H.
Albayati, Mustafa R.
author_facet Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Younes, Sabry H. H.
Albayati, Mustafa R.
author_sort Mague, Joel T.
collection PubMed
description In the title compound, C(16)H(12)N(2)O(3), the 2H-chromene moiety is essentially planar, with an r.m.s. deviation of the nine constituent atoms from the mean plane of 0.0093 Å, and makes a dihedral angle of 76.84 (3)° with the pendant phenyl ring. An intra­molecular N—H⋯O hydrogen bond helps to determine the conformation of the side chain. In the crystal, N—H⋯O and N—H⋯N hydrogen bonds link the mol­ecules, forming [100] chains.
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spelling pubmed-47199472016-02-11 Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide Mague, Joel T. Mohamed, Shaaban K. Akkurt, Mehmet Younes, Sabry H. H. Albayati, Mustafa R. Acta Crystallogr E Crystallogr Commun Data Reports In the title compound, C(16)H(12)N(2)O(3), the 2H-chromene moiety is essentially planar, with an r.m.s. deviation of the nine constituent atoms from the mean plane of 0.0093 Å, and makes a dihedral angle of 76.84 (3)° with the pendant phenyl ring. An intra­molecular N—H⋯O hydrogen bond helps to determine the conformation of the side chain. In the crystal, N—H⋯O and N—H⋯N hydrogen bonds link the mol­ecules, forming [100] chains. International Union of Crystallography 2015-11-28 /pmc/articles/PMC4719947/ /pubmed/26870466 http://dx.doi.org/10.1107/S2056989015022495 Text en © Mague et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Mague, Joel T.
Mohamed, Shaaban K.
Akkurt, Mehmet
Younes, Sabry H. H.
Albayati, Mustafa R.
Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title_full Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title_fullStr Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title_full_unstemmed Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title_short Crystal structure of 2-oxo-N′-phenyl-2H-chromene-3-carbohydrazide
title_sort crystal structure of 2-oxo-n′-phenyl-2h-chromene-3-carbohydrazide
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719947/
https://www.ncbi.nlm.nih.gov/pubmed/26870466
http://dx.doi.org/10.1107/S2056989015022495
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