Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde

The title compound, C(19)H(21)N(3)O, comprises a central pyrazole ring which is N-connected to an aldehyde group and C-connected twice to substituted benzene rings. The pyrazole ring is twisted on the C—C single bond, and the least-squares plane through this ring forms dihedral angles of 82.44 (5) a...

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Autores principales: Adam, Farook, Samshuddin, Seranthimata, Ameram, Nadiah, Subramaya, Samartha, Laxminarayana
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Data Reports
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719963/
https://www.ncbi.nlm.nih.gov/pubmed/26870482
http://dx.doi.org/10.1107/S2056989015023294
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author Adam, Farook
Samshuddin, Seranthimata
Ameram, Nadiah
Subramaya,
Samartha, Laxminarayana
author_facet Adam, Farook
Samshuddin, Seranthimata
Ameram, Nadiah
Subramaya,
Samartha, Laxminarayana
author_sort Adam, Farook
collection PubMed
description The title compound, C(19)H(21)N(3)O, comprises a central pyrazole ring which is N-connected to an aldehyde group and C-connected twice to substituted benzene rings. The pyrazole ring is twisted on the C—C single bond, and the least-squares plane through this ring forms dihedral angles of 82.44 (5) and 4.52 (5)° with the (di­methyl­amino)­benzene and p-tolyl rings, respectively. In the crystal, weak C—H⋯O hydrogen bonds link mol­ecules into supra­molecular tubes along the b axis.
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spelling pubmed-47199632016-02-11 Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde Adam, Farook Samshuddin, Seranthimata Ameram, Nadiah Subramaya, Samartha, Laxminarayana Acta Crystallogr E Crystallogr Commun Data Reports The title compound, C(19)H(21)N(3)O, comprises a central pyrazole ring which is N-connected to an aldehyde group and C-connected twice to substituted benzene rings. The pyrazole ring is twisted on the C—C single bond, and the least-squares plane through this ring forms dihedral angles of 82.44 (5) and 4.52 (5)° with the (di­methyl­amino)­benzene and p-tolyl rings, respectively. In the crystal, weak C—H⋯O hydrogen bonds link mol­ecules into supra­molecular tubes along the b axis. International Union of Crystallography 2015-12-09 /pmc/articles/PMC4719963/ /pubmed/26870482 http://dx.doi.org/10.1107/S2056989015023294 Text en © Adam et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Data Reports
Adam, Farook
Samshuddin, Seranthimata
Ameram, Nadiah
Subramaya,
Samartha, Laxminarayana
Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title_full Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title_fullStr Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title_full_unstemmed Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title_short Crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1H-pyrazole-1-carbaldehyde
title_sort crystal structure of 5-[4-(di­methyl­amino)­phen­yl]-3-(4-methyl­phen­yl)-4,5-di­hydro-1h-pyrazole-1-carbaldehyde
topic Data Reports
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4719963/
https://www.ncbi.nlm.nih.gov/pubmed/26870482
http://dx.doi.org/10.1107/S2056989015023294
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