Toward Structural Correctness: Aquatolide and the Importance of 1D Proton NMR FID Archiving

[Image: see text] The revision of the structure of the sesquiterpene aquatolide from a bicyclo[2.2.0]hexane to a bicyclo[2.1.1]hexane structure using compelling NMR data, X-ray crystallography, and the recent confirmation via full synthesis exemplify that the achievement of “structural correctness”...

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Detalles Bibliográficos
Autores principales: Pauli, Guido F., Niemitz, Matthias, Bisson, Jonathan, Lodewyk, Michael W., Soldi, Cristian, Shaw, Jared T., Tantillo, Dean J., Saya, Jordy M., Vos, Klaas, Kleinnijenhuis, Roel A., Hiemstra, Henk, Chen, Shao-Nong, McAlpine, James B., Lankin, David C., Friesen, J. Brent
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2016
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4746703/
https://www.ncbi.nlm.nih.gov/pubmed/26812443
http://dx.doi.org/10.1021/acs.joc.5b02456

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