Planning, performing and analyzing X-ray Raman scattering experiments

A compilation of procedures for planning and performing X-ray Raman scattering (XRS) experiments and analyzing data obtained from them is presented. In particular, it is demonstrated how to predict the overall shape of the spectra, estimate detection limits for dilute samples, and how to normalize t...

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Detalles Bibliográficos
Autores principales: Sahle, Ch. J., Mirone, A., Niskanen, J., Inkinen, J., Krisch, M., Huotari, S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4786055/
https://www.ncbi.nlm.nih.gov/pubmed/25723942
http://dx.doi.org/10.1107/S1600577514027581
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author Sahle, Ch. J.
Mirone, A.
Niskanen, J.
Inkinen, J.
Krisch, M.
Huotari, S.
author_facet Sahle, Ch. J.
Mirone, A.
Niskanen, J.
Inkinen, J.
Krisch, M.
Huotari, S.
author_sort Sahle, Ch. J.
collection PubMed
description A compilation of procedures for planning and performing X-ray Raman scattering (XRS) experiments and analyzing data obtained from them is presented. In particular, it is demonstrated how to predict the overall shape of the spectra, estimate detection limits for dilute samples, and how to normalize the recorded spectra to absolute units. In addition, methods for processing data from multiple-crystal XRS spectrometers with imaging capability are presented, including a super-resolution method that can be used for direct tomography using XRS spectra as the contrast. An open-source software package with these procedures implemented is also made available.
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spelling pubmed-47860552016-03-22 Planning, performing and analyzing X-ray Raman scattering experiments Sahle, Ch. J. Mirone, A. Niskanen, J. Inkinen, J. Krisch, M. Huotari, S. J Synchrotron Radiat Research Papers A compilation of procedures for planning and performing X-ray Raman scattering (XRS) experiments and analyzing data obtained from them is presented. In particular, it is demonstrated how to predict the overall shape of the spectra, estimate detection limits for dilute samples, and how to normalize the recorded spectra to absolute units. In addition, methods for processing data from multiple-crystal XRS spectrometers with imaging capability are presented, including a super-resolution method that can be used for direct tomography using XRS spectra as the contrast. An open-source software package with these procedures implemented is also made available. International Union of Crystallography 2015-02-03 /pmc/articles/PMC4786055/ /pubmed/25723942 http://dx.doi.org/10.1107/S1600577514027581 Text en © Ch. J. Sahle et al. 2015 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Sahle, Ch. J.
Mirone, A.
Niskanen, J.
Inkinen, J.
Krisch, M.
Huotari, S.
Planning, performing and analyzing X-ray Raman scattering experiments
title Planning, performing and analyzing X-ray Raman scattering experiments
title_full Planning, performing and analyzing X-ray Raman scattering experiments
title_fullStr Planning, performing and analyzing X-ray Raman scattering experiments
title_full_unstemmed Planning, performing and analyzing X-ray Raman scattering experiments
title_short Planning, performing and analyzing X-ray Raman scattering experiments
title_sort planning, performing and analyzing x-ray raman scattering experiments
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4786055/
https://www.ncbi.nlm.nih.gov/pubmed/25723942
http://dx.doi.org/10.1107/S1600577514027581
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