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Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials
In the present study, a novel approach for surface characterization of ceramic biomaterials is proposed. Two ceramic biomaterials—hydroxyapatite and β-tricalcium phosphate—were examined by means of inverse liquid chromatography. The Abraham LFER model was applied for physicochemical characteristics...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer Berlin Heidelberg
2016
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4803825/ https://www.ncbi.nlm.nih.gov/pubmed/27069275 http://dx.doi.org/10.1007/s10337-016-3049-5 |
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author | Adamska, Katarzyna Kadlec, Karol Voelkel, Adam |
author_facet | Adamska, Katarzyna Kadlec, Karol Voelkel, Adam |
author_sort | Adamska, Katarzyna |
collection | PubMed |
description | In the present study, a novel approach for surface characterization of ceramic biomaterials is proposed. Two ceramic biomaterials—hydroxyapatite and β-tricalcium phosphate—were examined by means of inverse liquid chromatography. The Abraham LFER model was applied for physicochemical characteristics of the surface. Different compounds, characterized by different polarity and different donor–acceptor properties of functional group, were used as test solutes. The chromatographic experiments were carried out with two compositions of the mobile phase: pure acetonitrile (MeCN) and the mixture of acetonitrile and water in 80:20 ratio (MeCN/H(2)O). Thus, the influence of mobile phase on sorption properties of hydroxyapatite and tricalcium phosphate surface was also discussed. |
format | Online Article Text |
id | pubmed-4803825 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2016 |
publisher | Springer Berlin Heidelberg |
record_format | MEDLINE/PubMed |
spelling | pubmed-48038252016-04-09 Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials Adamska, Katarzyna Kadlec, Karol Voelkel, Adam Chromatographia Original In the present study, a novel approach for surface characterization of ceramic biomaterials is proposed. Two ceramic biomaterials—hydroxyapatite and β-tricalcium phosphate—were examined by means of inverse liquid chromatography. The Abraham LFER model was applied for physicochemical characteristics of the surface. Different compounds, characterized by different polarity and different donor–acceptor properties of functional group, were used as test solutes. The chromatographic experiments were carried out with two compositions of the mobile phase: pure acetonitrile (MeCN) and the mixture of acetonitrile and water in 80:20 ratio (MeCN/H(2)O). Thus, the influence of mobile phase on sorption properties of hydroxyapatite and tricalcium phosphate surface was also discussed. Springer Berlin Heidelberg 2016-02-25 2016 /pmc/articles/PMC4803825/ /pubmed/27069275 http://dx.doi.org/10.1007/s10337-016-3049-5 Text en © The Author(s) 2016 Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. |
spellingShingle | Original Adamska, Katarzyna Kadlec, Karol Voelkel, Adam Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title | Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title_full | Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title_fullStr | Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title_full_unstemmed | Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title_short | Application of Inverse Liquid Chromatography for Surface Characterization of Biomaterials |
title_sort | application of inverse liquid chromatography for surface characterization of biomaterials |
topic | Original |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4803825/ https://www.ncbi.nlm.nih.gov/pubmed/27069275 http://dx.doi.org/10.1007/s10337-016-3049-5 |
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