Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene

In the title 1:1 co-crystal, C(12)H(10)N(2)·C(8)H(7)NO(4), the bi­pyridine moiety shows whole-mol­ecule disorder over two sets of sites in a 0.588 (3): 0.412 (3) ratio. In the crystal, the components form hydrogen-bonded sheets linked by N—H⋯O and O—H⋯N inter­actions, which stack along the a axis. A...

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Autores principales: McGuire, Scott C., Travis, Steven C., Tuohey, Daniel W., Deering, Thomas J., Martin, Bob, Cox, Jordan M., Benedict, Jason B.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2016
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4908539/
https://www.ncbi.nlm.nih.gov/pubmed/27308008
http://dx.doi.org/10.1107/S2056989016005259
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author McGuire, Scott C.
Travis, Steven C.
Tuohey, Daniel W.
Deering, Thomas J.
Martin, Bob
Cox, Jordan M.
Benedict, Jason B.
author_facet McGuire, Scott C.
Travis, Steven C.
Tuohey, Daniel W.
Deering, Thomas J.
Martin, Bob
Cox, Jordan M.
Benedict, Jason B.
author_sort McGuire, Scott C.
collection PubMed
description In the title 1:1 co-crystal, C(12)H(10)N(2)·C(8)H(7)NO(4), the bi­pyridine moiety shows whole-mol­ecule disorder over two sets of sites in a 0.588 (3): 0.412 (3) ratio. In the crystal, the components form hydrogen-bonded sheets linked by N—H⋯O and O—H⋯N inter­actions, which stack along the a axis. A comparison to a related and previously published co-crystal of 5-amino-isophthalic acid and the shorter 4,4′-bipryidine is presented.
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spelling pubmed-49085392016-06-15 Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene McGuire, Scott C. Travis, Steven C. Tuohey, Daniel W. Deering, Thomas J. Martin, Bob Cox, Jordan M. Benedict, Jason B. Acta Crystallogr E Crystallogr Commun Research Communications In the title 1:1 co-crystal, C(12)H(10)N(2)·C(8)H(7)NO(4), the bi­pyridine moiety shows whole-mol­ecule disorder over two sets of sites in a 0.588 (3): 0.412 (3) ratio. In the crystal, the components form hydrogen-bonded sheets linked by N—H⋯O and O—H⋯N inter­actions, which stack along the a axis. A comparison to a related and previously published co-crystal of 5-amino-isophthalic acid and the shorter 4,4′-bipryidine is presented. International Union of Crystallography 2016-04-08 /pmc/articles/PMC4908539/ /pubmed/27308008 http://dx.doi.org/10.1107/S2056989016005259 Text en © McGuire et al. 2016 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
McGuire, Scott C.
Travis, Steven C.
Tuohey, Daniel W.
Deering, Thomas J.
Martin, Bob
Cox, Jordan M.
Benedict, Jason B.
Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title_full Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title_fullStr Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title_full_unstemmed Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title_short Crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
title_sort crystal structure of the co-crystal of 5-amino­isophthalic acid and 1,2-bis(pyridin-4-yl)ethene
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4908539/
https://www.ncbi.nlm.nih.gov/pubmed/27308008
http://dx.doi.org/10.1107/S2056989016005259
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